二氯(1,2-丙烷二氨基)铂(II)合成路线 (共 5 条)
反应条件
HCl in water Pt-contg. compd. was dissolved in H2O and mixed with an equimolar amt. of the diamine ligand; pH was adjusted to ca. 3 (HCl); stirring at 80°C for 2 h; according to H. Hohmann, Inorg. Chim. Acta 174 (1990) 87; recrystn. from H2O; elem. anal.;
参考文献
Rajkovic, Snezana; Asanin, Darko P.; Zivkovic, Marija D.; Djuran, Milos I.
Polyhedron, 2013 , vol. 65, p. 42 - 47
反应条件
silver sulphate in water byproducts: AgI; Ag:Pt=1.28:0.65 molar ratio, Pt compd. added to a soln. of Ag salt, stirred overnight at 40°C in the dark, filtered, KCl (excess) added, stored for 24 h; ppt. centrifuged, washed (cold water, ethanol, diethyl ether), dried (vac.);
参考文献
Milanesio, Marco; Monti, Elena; Gariboldi, Marzia Bruna; Gabano, Elisabetta; Ravera, Mauro; Osella, Domenico
Inorganica Chimica Acta, 2008 , vol. 361, # 9-10 p. 2803 - 2814
反应条件
tetraethylammonium chloride; N(Et)4ClO4 in methanol Kinetics; at 25°C; monitored by UV (260-360 nm);
参考文献
Peloso, Arnaldo; Mohamud, Sacid Issa
Gazzetta Chimica Italiana, 1991 , vol. 121, # 7 p. 349 - 354
反应条件
in water formation on reaction of K2(PtCl4) with l-1,2-diaminopropane in aq. soln.;;
参考文献
Chugaev, L. A.; Sokolov, V.
Ber., 1907 , vol. 40, p. 3461 - 3465
反应条件
in methanol Kinetics; byproducts: Fe(C5H5)2(1+), Cl(1-); at 25-45°C; monitored by UV (280-400 nm);
参考文献
Peloso, Arnaldo; Mohamud, Sacid Issa
Gazzetta Chimica Italiana, 1991 , vol. 121, # 7 p. 349 - 354