2-苯基-2,3-二氢呋喃合成路线 (共 22 条)
反应条件
tetrabutyl-ammonium chloride; potassium acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide Ambient temperatureor 80 deg C;
参考文献
Larock, Richard C.; Gong, William H.; Baker, Bruce E.
Tetrahedron Letters, 1989 , vol. 30, # 20 p. 2603 - 2606
反应条件
Grubb's 2nd generation catalyst in dichloromethane T=45 - 70°C;
参考文献
Sutton, Amanda E.; Seigal, Benjamin A.; Finnegan, David F.; Snapper, Marc L.
Journal of the American Chemical Society, 2002 , vol. 124, # 45 p. 13390 - 13391
反应条件
N-ethyl-N,N-diisopropylamine; [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone in tetrahydrofuran T=50°C; Heck reaction; 15 h;
参考文献
Dieguez, Montserrat; Pamies, Oscar; Mata, Yvette; Teuma, Emmanuelle; Gomez, Montserrat; Ribaudo, Fabrizio; Van Leeuwen, Piet W. N. M.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 16 p. 2583 - 2598
反应条件
[Ru(N,N-bis[(pyridin-2-yl)methyl][2-(diphenylphosphino)phenyl]methanamine)(CH3COO)][BPh4] in tetrahydrofuran T=80°C; 17 h; Inert atmosphere;
参考文献
Liu, Fei Nian; Su, Fu Hai; Wen, Ting Bin; Sung, Herman H.-Y.; Williams, Ian D.; Jia, Guochen
Chemistry - A European Journal, 2010 , vol. 16, # 26 p. 7889 - 7897
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; N-ethyl-N,N-diisopropylamine; tris(dibenzylideneacetone)dipalladium (0) in N,N-dimethyl-formamide T=150°C; 0.5 h; microwave irradiation;
参考文献
Arshad, Nuzhat; Hashim, Jamshed; Kappe, C. Oliver
Journal of Organic Chemistry, 2008 , vol. 73, # 12 p. 4755 - 4758
反应条件
N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); (S)-2-[2-(diphenylphosphino)benzyl]-4-iso-propyl-4,5-dihydrooxazole in tetrahydrofuran T=60°C; Heck reaction; 20 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Henriksen, Signe T.; Norrby, Per-Ola; Kaukoranta, Paeivi; Andersson, Pher G.
Journal of the American Chemical Society, 2008 , vol. 130, # 31 p. 10414 - 10421
反应条件
potassium phosphate; 1'-carbopalladated ferrocene in N,N-dimethyl acetamide T=80°C; Heck coupling; 3 h;
参考文献
Hillers, Stephan; Reiser, Oliver
Tetrahedron Letters, 1993 , vol. 34, # 33 p. 5265 - 5268
反应条件
tris-(dibenzylideneacetone)dipalladium(0); C26H24NPS; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=120°C; Heck reaction; 4 h; Microwave irradiation; optical yield given as percent eeenantioselective reaction;
参考文献
Henriksen, Signe T.; Norrby, Per-Ola; Kaukoranta, Paeivi; Andersson, Pher G.
Journal of the American Chemical Society, 2008 , vol. 130, # 31 p. 10414 - 10421
反应条件
N-ethyl-N,N-diisopropylamine; 4,5-bis[(2R,5R)-2,5-dimethylphospholanyl]-9,9-dimethylxanthene; bis(dibenzylideneacetone)-palladium(0) in benzene Heck reaction; 48 h; Heating;
参考文献
Malaise, Gregory; Ramdeehul, Shailesh; Osborn, John A.; Barloy, Laurent; Kyritsakas, Nathalie; Graff, Roland
European Journal of Inorganic Chemistry, 2004 , # 20 p. 3987 - 4001
反应条件
ethyl vinyl ether in toluene T=20 - 110°C; Inert atmosphere;
参考文献
Schmidt, Bernd; Geissler, Diana
European Journal of Organic Chemistry, 2011 , # 25 p. 4814 - 4822