1-叔丁基-3-甲氧基苯合成路线 (共 24 条)
反应条件
nitric acid; acetic anhydride
参考文献
Carpenter et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 586,606
反应条件
1: 3-tert-butyl-1-methoxybenzene With hydrogenchloride; N-bromosuccinmide; water in acetone
T=20°C; 0.0833333 h; Inert atmosphere;
2: With tert.-butyl lithium in tetrahydrofuran; pentane
T=-78°C; 0.5 h; Inert atmosphere;
3: N,N-dimethyl-formamide in tetrahydrofuran; pentane
T=-78 - 20°C; Inert atmosphere;
参考文献
Tietze, Lutz F.; Vock, Carsten A.; Krimmelbein, Ilga K.; Nacke, Linda
Synthesis, 2009 , # 12 art. no. T20108SS, p. 2040 - 2060
参考文献
Iwata,M.; Emoto,S.
Bulletin of the Chemical Society of Japan, 1974 , vol. 47, p. 1687 - 1692
反应条件
sulfuric acid; nitric acid
参考文献
Carpenter et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 586,606