反应条件
carbon monoxide; sulfuric acid; triphenylphosphine in butan-1-ol byproducts: Na2SO4, H2O, CO2; (inert atm.); Pd(OAc)2 and PPh3 stirred (10-15 min); H2SO4 added; stream of CO was intriduced (1.5-2 h); Pd(PPh3)4 filtered off; filtrate treated with 1 N NaOH; ppt. filtered; washed (water, ethanol, hexane); dried (vac.); elem. anal.;
参考文献
Min'kov, A. I.; Eremenko, N. K.; Merkur'eva, S. E.; Efimov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 6 p. 1223 - 1226
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 6 p. 1347 - 1351
