N-甲基-1-苯基甲亚胺氧化物合成路线 (共 74 条)
反应条件
1: 98 percent 2: 98 percent / MCPBA / CH2Cl2 / 12 h / 25 °C View Scheme
参考文献
Padwa, Albert; Kline, Donald N.; Perumattam, John
Tetrahedron Letters, 1987 , vol. 28, # 9 p. 913 - 916
反应条件
in benzene 240 h; Heating; Yield given;
参考文献
Tetrahedron, , vol. 37, p. 1349 - 1357
反应条件
in benzene 480 h; Ambient temperature; Yield given;
参考文献
Cristina, D.; Amici, M. De; Micheli, C. De; Gandolfi, R.
Tetrahedron, 1981 , vol. 37, p. 1349 - 1357
反应条件
1: benzene / 20 h / Heating 2: 72 percent 3: 94 percent / TiCl3, AcOH, AcONa / Ambient temperature 4: Raney Ni / ethanol / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 20 p. 4004 - 4005
反应条件
2: 1.) LDA 2.) γ-alkylation 3: 91 percent / MCPBA / CH2Cl2 / 12 h / 25 °C 4: Al(Hg) View Scheme
参考文献
Padwa, Albert; Kline, Donald N.; Perumattam, John
Tetrahedron Letters, 1987 , vol. 28, # 9 p. 913 - 916
反应条件
in dichloromethane T=80°C; 12 h; Sealed tube;
参考文献
Lasri, Jamal; Gajewski, Grzegorz; Guedes Da Silva, M. Fatima C.; Kuznetsov, Maxim L.; Fernandes, Ricardo R.; Pombeiro, Armando J.L.
Tetrahedron, 2012 , vol. 68, # 35 p. 7019 - 7027
反应条件
trifluoroacetic anhydride; sodium iodide in acetonitrile T=20°C; var. nitrones; Product distribution;
参考文献
Balicki, Roman
Gazzetta Chimica Italiana, 1990 , vol. 120, # 1 p. 67 - 68
反应条件
9,10-anthracenedicarbonitrile in acetonitrile 1 h; Irradiationother arylnitrones, other solvent and time; Product distribution;
参考文献
Chemistry Letters, , # 4 p. 707 - 710
反应条件
in benzene T=190°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Niwayama, Satomi; Dan, Shigeyuki; Inouye, Yoshinobu; Kakisawa, Hiroshi
Chemistry Letters, 1985 , p. 957 - 960
反应条件
in dichloromethane T=80°C; 12 h; Sealed tube;
参考文献
Lasri, Jamal; Gajewski, Grzegorz; Guedes Da Silva, M. Fatima C.; Kuznetsov, Maxim L.; Fernandes, Ricardo R.; Pombeiro, Armando J.L.
Tetrahedron, 2012 , vol. 68, # 35 p. 7019 - 7027