N-甲基-1-苯基甲亚胺氧化物合成路线 （共 74 条）
反应条件
1: tetrahydrofuran / 20 °C 2: 100 percent / In; sat. aq. NH4Cl / ethanol / 4 h / Heating View Scheme
参考文献
Cicchi, Stefano; Bonanni, Marco; Cardona, Francesca; Revuelta, Julia; Goti, Andrea
Organic Letters, 2003 , vol. 5, # 10 p. 1773 - 1776
反应条件
mercury(II) oxide in chloroform-d1 T=0°C; Isomerization; Kinetics;
参考文献
Hassan, Azfar; Wazeer, Mohammed I. M.; Saeed, Mohammed T.; Siddiqui, Mohammad N.; Ali, Sk. Asrof
Journal of Physical Organic Chemistry, 2000 , vol. 13, # 8 p. 443 - 451
反应条件
in benzene 240 h; Heating; Yield given;
参考文献
Cristina, D.; Amici, M. De; Micheli, C. De; Gandolfi, R.
Tetrahedron, 1981 , vol. 37, p. 1349 - 1357
参考文献
Prajapati, Dipak; Sandhu, J. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 8 p. 758
反应条件
1: 21 h / 110 °C 2: LiAlH4 / diethyl ether View Scheme
参考文献
Huisgen,R. et al.
Chemische Berichte, 1968 , vol. 101, # 7 p. 2568 - 2584
反应条件
triethylamine in 1,4-dioxane
8 h; Yield given;
参考文献
Roux, Maria Victoria; Jimenez, Pilar; Martin-Luengo, Maria Angeles; Davalos, Juan Z.; Sun, Zhiyuan; Hosmane, Ramachandra S.; Liebman, Joel F.
Journal of Organic Chemistry, 1997 , vol. 62, # 9 p. 2732 - 2737
反应条件
4 A molecular sieve; nickel(II) chlorate(VII) in ethylene glycol dimethyl ether
T=-40°C; 30 h; Title compound not separated from byproducts.;
参考文献
Kang, Yan-Biao; Sun, Xiu-Li; Tang, Yong
Angewandte Chemie - International Edition, 2007 , vol. 46, # 21 p. 3918 - 3921
反应条件
in dichloromethane
T=80°C; 2 h; Sealed tube;
参考文献
Lasri, Jamal; Gajewski, Grzegorz; Guedes Da Silva, M. Fatima C.; Kuznetsov, Maxim L.; Fernandes, Ricardo R.; Pombeiro, Armando J.L.
Tetrahedron, 2012 , vol. 68, # 35 p. 7019 - 7027
反应条件
in dichloromethane
T=20 - 80°C; 4 h; Sealed tube;
参考文献
Lasri, Jamal
Letters in Organic Chemistry, 2013 , vol. 10, # 7 p. 482 - 489
反应条件
1.) toluene, 80 deg C, 22 h, 2.) xylene, reflux, 25 h; Yield given. Multistep reaction;
参考文献
Tanaka, Kiyoshi; Mori, Takami; Mitsuhashi, Keiryo
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 1 p. 263 - 268
