N-甲基-1-苯基甲亚胺氧化物合成路线 (共 74 条)
反应条件
1.) 60 deg C, 2d, 2.) 400 deg C, 0.15 Torr; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brandi; Garro; Guarna; Goti; Cordero; De Sarlo
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2430 - 2434
反应条件
potassium cyanide in ethanol
参考文献
Cawkill, Eric; Clark, Nigel G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 244 - 248
反应条件
in ethanol; water
Ambient temperatureother N-(substituted benzylidene)methylamine N-oxides; Mechanism;
参考文献
Soni, R. P.
Australian Journal of Chemistry, 1982 , vol. 35, # 7 p. 1493 - 1496
反应条件
in benzene
8 h; Heating;
参考文献
Harpp, David N.; MacDonald, J. Gavin; Larsen, Charles
Canadian Journal of Chemistry, 1985 , vol. 63, p. 951 - 957
反应条件
1,1'-carbonothioylbis-1H-imidazole in benzene
Heating;
参考文献
Harpp, David N.; MacDonald J. Gavin
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 4927 - 4930
反应条件
in benzene
36 h; Heating;
参考文献
Baruah, Arpan K.; Prajapati, Dipak; Sandhu, Jagir S.
Tetrahedron, 1988 , vol. 44, # 19 p. 6137 - 6142
反应条件
in benzene
8 h; Ambient temperature;
参考文献
Harpp, David N.; MacDonald, J. Gavin; Larsen, Charles
Canadian Journal of Chemistry, 1985 , vol. 63, p. 951 - 957
反应条件
in benzene
40 h; Heating; Yield given;
参考文献
Sain, Bir; Prajapati, Dipak; Mahajan, Asha R; Sandhu, Jagir S
Bulletin de la Societe Chimique de France, 1994 , vol. 131, # 3 p. 313 - 316
反应条件
in dichloromethane
T=80°C; 2 h; Sealed tube;
参考文献
Lasri, Jamal; Gajewski, Grzegorz; Guedes Da Silva, M. Fatima C.; Kuznetsov, Maxim L.; Fernandes, Ricardo R.; Pombeiro, Armando J.L.
Tetrahedron, 2012 , vol. 68, # 35 p. 7019 - 7027
反应条件
1: 45 percent / cathecol / toluene / 192 h / 120 °C
2: 93 percent / 0.5 h / 160 °C
3: 82 percent / NaH / tetrahydrofuran / 9 h / 65 °C
View Scheme
参考文献
Chiacchio, Ugo; Liguori, Angelo; Romeo, Giovanni; Sindona, Giovanni; Uccella, Nicola
Heterocycles, 1993 , vol. 36, # 4 p. 799 - 817