反应条件
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / Inert atmosphere 1.2: 16 h / Inert atmosphere 2.1: hydrogenchloride; acetic acid; zinc / water / 16 h / Inert atmosphere 3.1: aluminium hydride / toluene / 4.33 h / -78 - 20 °C / Inert atmosphere 3.2: 0.17 h / 0 °C / Inert atmosphere 4.1: tri-n-butyl-tin hydride; 1,1'-azobis (cyclohexanecarbonitrile) / toluene / 65 h / Inert atmosphere; Reflux View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 13 p. 4882 - 4885