1,10-菲罗啉-2-甲醛合成路线 （共 5 条）
反应条件
Dess-Martin periodane in dichloromethane T=55°C; Dess-Martin reaction; 8 h;
参考文献
Luecking; Chen; Rudkevich; Rebek Jr.
Journal of the American Chemical Society, 2001 , vol. 123, # 41 p. 9929 - 9934
反应条件
selenium(IV) oxide in 1,4-dioxane 2 h; Reflux;
参考文献
Zhang, Min; Gao, Rong; Hao, Xiang; Sun, Wen-Hua
Journal of Organometallic Chemistry, 2008 , vol. 693, # 26 p. 3867 - 3877
反应条件
1.1: sodium / 0.5 h / Heating 1.2: 62 percent / aq. HCl / 0.5 h / 0 °C 2.1: 91 percent / sodium borohydride / ethanol / 48 h / 20 °C 3.1: 71 percent / selenium dioxide / dioxane / 2 h / Heating View Scheme
参考文献
Weijnen, John G. F.; Koudijs, Arie; Engbersen, Johan F. J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , p. 1121 - 1126
反应条件
1: 91 percent / sodium borohydride / ethanol / 48 h / 20 °C 2: 71 percent / selenium dioxide / dioxane / 2 h / Heating View Scheme
参考文献
Weijnen, John G. F.; Koudijs, Arie; Engbersen, Johan F. J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , p. 1121 - 1126
反应条件
sodium tetrahydroborate in ethanol
2.5 h; Heating;
参考文献
Holan, George; Wernert, Gregory T.
Australian Journal of Chemistry, 1987 , vol. 40, # 5 p. 873 - 881
