n,n-二甲基亚甲基碘化胺合成路线 (共 57 条)
反应条件
sodium hydroxide
1.) THF, RT, 3 h, 2.) THF, 20 min; Yield given. Multistep reaction;
参考文献
Hooz, John; Oudenes, Jan; Roberts, J. L.; Benderly, Abraham
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1347 - 1349
反应条件
in acetic acid; acetonitrile
T=20°C; 3 h;
参考文献
Soto, Sara; Vaz, Esther; Dell'Aversana, Carmela; Alvarez, Rosana; Altucci, Lucia; De Lera, Angel R.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 10 p. 2101 - 2112
反应条件
potassium carbonate in dichloromethane
7 h; Ambient temperature;
参考文献
Pochini, Andrea; Puglia, Giuseppe; Ungaro, Rocco
Synthesis, 1983 , # 11 p. 906 - 907
反应条件
potassium carbonate in toluene
4 h; Ambient temperature;
参考文献
Pochini, Andrea; Puglia, Giuseppe; Ungaro, Rocco
Synthesis, 1983 , # 11 p. 906 - 907
反应条件
potassium carbonate in dichloromethane
0.5 h; Ambient temperature;
参考文献
Anwar, Hany F.; Skattebol, Lars; Hansen, Trond Vidar
Tetrahedron, 2007 , vol. 63, # 40 p. 9997 - 10002
参考文献
Le Notre, Jerome; Van Mele, David; Frost, Christopher G.
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 3 p. 432 - 440
反应条件
in acetic acid; acetonitrile
T=20°C; 2 h;
参考文献
Ley, Steven V.; Priour, Alain
European Journal of Organic Chemistry, 2002 , # 23 p. 3995 - 4004