2-氯-1,1-二氟乙烷合成路线 （共 23 条）
反应条件
thionyl chloride T=0 - 35°C;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY; PETROV, Viacheslav, A.; DUBOIS, Charles, J.
Patent: WO2013/180782 A1, 2013 ;
Location in patent: Page/Page column 35; 36; 37 ;
反应条件
hydrogen fluoride; mercury(II) oxide T=95°C; im Autoklaven;
参考文献
Henne; Renoll
Journal of the American Chemical Society, 1936 , vol. 58, p. 890
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McBee; Bolt
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 412,413
反应条件
fluorine an einem Kupferdrahtnetz;
参考文献
Calfee et al.
Journal of the American Chemical Society, 1940 , vol. 62, p. 267
反应条件
1: in dichloromethane T=60°C; Addition; 18 h; 2: With tri-n-butyl-tin hydride Reduction;
参考文献
Kharroubi; Manseri; Ameduri; Boutevin
Journal of Fluorine Chemistry, 2000 , vol. 103, # 2 p. 145 - 153
反应条件
1: With hydrogen fluoride; chromium - based fluorination catalyst T=180°C; 2: With Cr and In on graphite catalyst T=180°C; 4 h; Inconel 600 type reactor; 3: With Cr on active alumina catalyst Inconel 600 type reactor; Product distribution / selectivity;
参考文献
SHOWA DENKO K.K.
Patent: WO2005/92823 A2, 2005 ;
Location in patent: Page/Page column 10-16 ;
反应条件
diethylamino-sulfur trifluoride in tetrachloromethane Ambient temperature;
参考文献
Siegemund,G.
Liebigs Annalen der Chemie, 1979 , p. 1280 - 1290
反应条件
in dichloro difluoro methane 1.) -150 deg C to -30 deg C, 24 h; 2.) -30 deg C to 22 deg C, 0.2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Johri, Kamalesh K.; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 242 - 250
反应条件
T=140°C; unter Druck;
参考文献
Henne; Renoll
Journal of the American Chemical Society, 1936 , vol. 58, p. 890
Full Text Show Details
Henne; Midgley
Journal of the American Chemical Society, 1936 , vol. 58, p. 886
参考文献
Henne; Renoll
Journal of the American Chemical Society, 1936 , vol. 58, p. 890
参考文献
Henne; Renoll
Journal of the American Chemical Society, 1936 , vol. 58, p. 890
