N-苯基-1,2,3,4-四氢-2-氨基萘合成路线 (共 6 条)
反应条件
1: With acetic acid T=20 - 35°C; 0.25 h; 2: With sodium tris(acetoxy)borohydride in 1,2-dichloro-ethane T=20 - 40°C; 3: With sodium hydroxide; water in 1,2-dichloro-ethane
参考文献
BRIDGE PHARMA, INC.
Patent: WO2008/11161 A2, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
benzo[1,3,2]dioxaborole in ethanol; water; toluene-4-sulfonic acid hydrazide
参考文献
A. Christiaens Societe Anonyme
Patent: US3970650 A1, 1976 ;
反应条件
nickel T=100 - 150°C; P=73550.8 - 147102 Torr; Hydrogenation;
参考文献
Wingfoot Corp.
Patent: US2095897 , 1936 ;
反应条件
nickel T=100 - 150°C; P=147102 Torr; Hydrogenation;
参考文献
Wingfoot Corp.
Patent: US2109165 , 1932 ;
反应条件
hydrogenchloride in 1,4-dioxane; diethyl ether
参考文献
BRIDGE PHARMA, INC.
Patent: WO2008/11161 A2, 2008 ;
Location in patent: Page/Page column 12 ;
参考文献
A. Christiaens, Societe Anonyme
Patent: US3943172 A1, 1976 ;