6,7-二甲氧基-3,4-二氢异喹啉合成路线 (共 75 条)
反应条件
1: 73 percent / H2, HCl / 5percent Pd-C / ethanol / 24 h / 760 Torr / Ambient temperature 2: 80 percent / HCO2H 3: t-butyl hydroperoxide / RuCl2(PPh3)3 View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 4 p. 1252 - 1254
反应条件
2,2'-azo-bisisobutyronitrile; n-Bu3SnD in toluene Decomposition; deuterium incorporation; 4 h; Heating;
参考文献
Organic Letters, , vol. 2, # 3 p. 307 - 310
反应条件
formic acid Pictet-Spengler reaction; 1 h; Heating;
参考文献
Heterocycles, , vol. 55, # 8 p. 1569 - 1580
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 18 h; Heating;
参考文献
Estevez, Juan C.; Villaverde, M. Carmen; Estevez, Ramon J.; Castedo, Luis
Tetrahedron, 1991 , vol. 50, # 7 p. 2107 - 2114
反应条件
sodium perchlorate in acetonitrile anode potential 0.95 - 1.1 V;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 833 - 837
反应条件
trichlorophosphate T=190 - 200°C; 2.5 h; Yield given;
参考文献
Chemische Berichte, , vol. 117, # 4 p. 1436 - 1454
参考文献
Zou, Zhi-Hong; Lan, Xiao-Bu; Qian, Hai; Huang, Wen-Long; Li, Yun-Man
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 19 p. 5934 - 5938
参考文献
Helvetica Chimica Acta, , vol. 41, p. 119,129
Chemical and Pharmaceutical Bulletin, , vol. 10, p. 185,186, 189
参考文献
Helvetica Chimica Acta, , vol. 41, p. 119,129
Chemical and Pharmaceutical Bulletin, , vol. 10, p. 185,186, 189
反应条件
2: sodium ethylate; benzene 3: aqueous hydrochloric acid View Scheme
参考文献
Helvetica Chimica Acta, , vol. 41, p. 119,129