3,5-二叔丁基邻苯醌合成路线 （共 229 条）
反应条件
in benzene byproducts: HCl; in refluxing benzene, HCl removed by distn. off,; anal., 41percent starting germane, 37percent quinone left;
参考文献
Journal of Organometallic Chemistry, , vol. 339, p. 51 - 60
反应条件
acetaldehyde in benzene Irradiation; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 11 p. 3657 - 3658
反应条件
in benzene byproducts: HCl; 12 h at 60 ° C in a sealde tube, concn. under reduced pressure; anal.; 38percent starting germane left;
参考文献
Journal of Organometallic Chemistry, , vol. 339, p. 51 - 60
反应条件
in benzene byproducts: HCl; heating in a sealed tube at 80 ° C for 12 h,; concn. (reduced pressure), anal. (IR, H-NMR, MS); 13percent starting germane;
参考文献
Journal of Organometallic Chemistry, , vol. 339, p. 51 - 60
反应条件
in benzene-d6 T=24.84°C; Irradiation;
参考文献
Shurygina; Kurskii; Chesnokov; Druzhkov; Fukin; Abakumov; Cherkasov
Russian Chemical Bulletin, 2006 , vol. 55, # 9 p. 1585 - 1592
反应条件
in benzene-d6 T=24.84°C; Irradiation;
参考文献
Shurygina; Kurskii; Chesnokov; Druzhkov; Fukin; Abakumov; Cherkasov
Russian Chemical Bulletin, 2006 , vol. 55, # 9 p. 1585 - 1592
反应条件
water in toluene byproducts: LiH; addn. of quinone in toluene to a soln. of Ge-compd., standing for 24 h at 20°C, rapid hydrolysis; extn. with ether, concn. and drying over Na2SO4, concn. under reduced pressure, analysis with GLC, NMR;
参考文献
Riviere, P.; Castel, A.; Ko, Y. H.; Desor, D.
Journal of Organometallic Chemistry, 1990 , vol. 386, # 2 p. 147 - 156
反应条件
in benzene inert atmosphere; heating (ampoule fused, 80°C, 48 h); further products;
参考文献
Journal of Organometallic Chemistry, , vol. 443, # 1 p. 43 - 49
反应条件
in benzene Irradiation; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 11 p. 3657 - 3658
反应条件
in chlorobenzene T=25°C; Irradiationother amines, other solvents; Rate constant;
参考文献
Chesnokov; Cherkasov; Abakumov; Kurskii; Shurygina; Mamysheva; Shavyrin
Russian Chemical Bulletin, 2003 , vol. 52, # 3 p. 718 - 724
