3,5-二叔丁基邻苯醌合成路线 （共 229 条）
反应条件
ascorbic acid powder in methanol Rate constant;
参考文献
Jovanovic, S. V.; Konya, K.; Scaiano, J. C.
Canadian Journal of Chemistry, 1995 , vol. 73, p. 1803 - 1810
反应条件
1: 63 percent Spectr. / benzene / Ambient temperature 2: 2N H2SO4 / tetrahydrofuran / 65 °C View Scheme
参考文献
Knaap, Th. A. van der; Bickelhaupt, F.
Tetrahedron, 1983 , vol. 39, # 19 p. 3189 - 3196
反应条件
in toluene N2 atmosphere; addn. of soln. of benzoquinone to suspn. of SnI2 (dropwise), refluxig (4 h), addn. of bipyridine, pptn., refluxing (1 h), cooling (room temp.); filtration off, washing (light petroleum), drying (vac.); elem. anal., IR spectroscopy;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 439 - 446
反应条件
acetic anhydride 24 h; Ambient temperature;
参考文献
Nicolaides, Demetrios N.; Adamopoulos, Spyros G.; Lefkaditis, Demetrios A.; Litinas, Konstantinos E.; Tarantili, Petroula V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 2 p. 283 - 290
反应条件
in benzene-d6 (high vacuum system), 12h at 120°C; detected by NMR, GC/MS;
参考文献
Journal of Organometallic Chemistry, , vol. 315, p. 157 - 164
反应条件
in benzene byproducts: HCl; in refluxing benzene, HCl removed by distn. off,; anal., 41percent starting germane, 37percent quinone left;
参考文献
Journal of Organometallic Chemistry, , vol. 339, p. 51 - 60
参考文献
Barrau, J.; Hamida, N. Ben
Inorganica Chimica Acta, 1990 , vol. 175, p. 159 - 160
参考文献
Barrau, J.; Hamida, N. Ben
Inorganica Chimica Acta, 1990 , vol. 175, p. 159 - 160
反应条件
in solid matrix 2-chlorobutane glass contg. Mn2(CO)9 and excess of quinone warmed to 220 K; not isolated, IR;
参考文献
Graaf, T. van der; Stufkens, D. J.; Vichova, J.; Vlcek, A.
Journal of Organometallic Chemistry, 1991 , vol. 401, # 3 p. 305 - 330
反应条件
in benzene inert atmosphere; heating (ampoule fused, 80°C, 48 h); further products;
参考文献
Journal of Organometallic Chemistry, , vol. 443, # 1 p. 43 - 49
