1,2,4,5-四苯基苯合成路线 （共 36 条）
反应条件
in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Harada, Katsumasa; Hart, Harold; Du, Chi-Jen Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5524 - 5528
反应条件
potassium fluoride; palladium diacetate Suzuki coupling reaction; 0.116667 h; microwave irradiation;
参考文献
Basu, Basudeb; Das, Pralay; Bhuiyan, Md. Mosharef H.; Jha, Satadru
Tetrahedron Letters, 2003 , vol. 44, # 19 p. 3817 - 3820
参考文献
Toda, Takashi; Tokida, Akihiko; Mukai, Toshio; Suzuki, Yoshizo
Chemistry Letters, 1981 , p. 1535 - 1538
反应条件
1: 92 percent / bromine, iron, iodine, oleum (29percent SO3) / 6 h / 60 - 70 °C 2: 1.) Mg / 1.) THF, 2.) THF, RT, 12 h View Scheme
参考文献
Harada, Katsumasa; Hart, Harold; Du, Chi-Jen Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5524 - 5528
反应条件
1: AgClO4 / acetonitrile 2: (heating) View Scheme
参考文献
Weiss,R.; Schlierf,C.
Angewandte Chemie, 1971 , vol. 83, p. 887 - 888
反应条件
1: HBr, FeCl3 / acetic acid 2: KOH View Scheme
参考文献
Staab,H.A.; Kurmeier,H.-A.
Chemische Berichte, 1968 , vol. 101, # 8 p. 2697 - 2708
反应条件
in diethyl ether 1.) RT, 24 h, 2.) reflux, 1 h;
参考文献
Saednya, Akbar; Hart, Harold
Synthesis, 1996 , # 12 p. 1455 - 1458
反应条件
in hexane under protective gas, to suspn. of Ir complex in n-hexane added at 20°C with stirring C2Ph2, allowed to stand for ca. 15 h; concd., chromd. (Al2O3/5percent H2O, at -10°C, n-hexane), concd., crystd. at -78°C; elem. anal.;
参考文献
Mueller, Joern; Passon, Barbara; Pickardt, Joachim
Journal of Organometallic Chemistry, 1982 , vol. 236, # 1 p. C11 - C14
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane 120 h; RefluxInert atmosphere; Overall yield = 96 percent;
参考文献
Ajaz, Aida; McLaughlin, Erin C.; Skraba, Sarah L.; Thamatam, Rajesh; Johnson, Richard P.
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9487 - 9495
反应条件
hydrogenchloride; phenyl-magnesium bromide 1.) THF, RT, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Harada, Katsumasa; Hart, Harold; Du, Chi-Jen Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5524 - 5528
