反应条件
1.1: sulfuryl dichloride / dichloromethane / 1 h / 0 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C / Inert atmosphere
2.2: 20 h / 0 - 23 °C / Inert atmosphere
3.1: boron trifluoride diethyl etherate / dichloromethane / 0 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
