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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
338396-06-8
合成路线
（共 11 条）
338396-06-8
+
355408-55-8
噻吩-2-硼酸新戊二醇酯
→
反应条件
17595-86-7
4-噻吩-2-硼酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
905966-46-3
+
338396-06-8
→
反应条件
20608-91-7
4-(3-噻吩基)苯甲酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
905966-40-7
+
338396-06-8
→
反应条件
792-74-5
联苯-4,4-二羧酸二甲酯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
338396-06-8
→
反应条件
55676-77-2
[1,1’-联苯]-2,4’-二甲酸二乙酯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 14 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
338396-06-8
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
338396-06-8
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki coupling; Inert atmosphere;
参考文献
Chen, Guo-Jun; Han, Fu-She
European Journal of Organic Chemistry, 2012 , # 19 p. 3575 - 3579
338396-06-8
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 8 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
338396-06-8
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
338396-06-8
+
98-80-6
苯硼酸
→
反应条件
720-75-2
联苯-4-羧酸甲酯
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki coupling; Inert atmosphere;
参考文献
Chen, Guo-Jun; Han, Fu-She
European Journal of Organic Chemistry, 2012 , # 19 p. 3575 - 3579
338396-06-8
+
5123-13-7
5,5-二甲基-2-苯基-1,3,2-二氧硼杂
→
反应条件
720-75-2
联苯-4-羧酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
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