2-(碘甲基)-6-[(苯基甲氧基)甲基]-1,4-二恶烷合成路线 （共 7 条）
反应条件
iodine; sodium hydrogencarbonate in diethyl ether; water T=0°C; 3 h;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
N-iodo-succinimide in acetonitrile T=20°C;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
N-iodo-succinimide in acetonitrile 3 h; Heating;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
1: 88 percent / NaH / 4 h / 20 °C 2: 8 percent / I2; NaHCO3 / H2O; diethyl ether / 3 h / 0 °C View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
1: 88 percent / NaH / 4 h / 20 °C 2: 8 percent / I2; NaHCO3 / H2O; diethyl ether / 3 h / 0 °C View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
18-crown-6 ether in N,N-dimethyl-formamide T=80°C; 24 h;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
1: 63 percent / 18-crown-6 / dimethylformamide / 24 h / 80 °C
2: 90 percent / HCl / methanol / 20 °C
View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
