(2-氧代-2-苯基乙基)苯甲酸酯合成路线 (共 39 条)
反应条件
8-methylquinoline 1-oxide; Au(Ph3P)+NTf2- in chlorobenzene T=20°C; 8 h;
参考文献
Wu, Chao; Liang, Zhiwu; Yan, Dong; He, Weimin; Xiang, Jiannan
Synthesis (Germany), 2013 , vol. 45, # 18 art. no. SS-2013-H0349-OP, p. 2605 - 2611
反应条件
pyridine in dichloromethane T=0°C;
参考文献
Trost, Barry M.; Xu, Jiayi; Reichle, Markus
Journal of the American Chemical Society, 2007 , vol. 129, # 2 p. 282 - 283
反应条件
N-bromosuccinmide; oxygen; 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride; triethylamine in dimethyl sulfoxide T=25°C; P=760.051 Torr; 38 h; regioselective reaction;
参考文献
Reddi, Rambabu N.; Malekar, Pushpa V.; Sudalai, Arumugam
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 38 p. 6477 - 6482
反应条件
1: With ozone in dichloromethane T=-78°C; 2: With triethylamine in dichloromethane T=-78 - 20°C; 6 h;
参考文献
Hon, Yung-Son; Wong, Ying-Chieh; Wu, Kuo-Jui
Journal of the Chinese Chemical Society, 2008 , vol. 55, # 4 p. 896 - 914
反应条件
dibenzo-18-crown-6; tetrabutylammomium bromide in acetonitrile 0.75 h; Ambient temperatureother conditions;
参考文献
Jugdale; Patil; Salunkhe
Synthetic Communications, 1996 , vol. 26, # 9 p. 1747 - 1752
反应条件
8-methylquinoline 1-oxide; C33H48AuClNP in chlorobenzene T=20°C; 12 h;
参考文献
Ji, Kegong; Zhao, Yulong; Zhang, Liming
Angewandte Chemie - International Edition, 2013 , vol. 52, # 25 p. 6508 - 6512
Angew. Chem., 2013 , vol. 125, # 25 p. 6636 - 6640
反应条件
potassium carbonate in acetonitrile room temperature, 20 min -> reflux, 50 min;
参考文献
Huang, Zhizhen; Xie, Linghong; Huang, Xian
Synthetic Communications, 1988 , vol. 18, # 10 p. 1167 - 1170
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate T=20°C; 0.25 h;
参考文献
Liu, Zhi; Chen, Zhen-Chu; Zheng, Qin-Guo
Synthesis, 2004 , # 1 p. 33 - 36
反应条件
manganese triacetate in benzene 48 h; Heating;
参考文献
Demir, Ayhan S.; Camkerten, Nurettin; Akgun, Hulya; Tanyeli, Cihangir; Mahasneh, Ali S.; Watt, David S.
Synthetic Communications, 1990 , vol. 20, # 15 p. 2279 - 2289
反应条件
potassium carbonate in acetonitrile T=60°C; Darzens type reaction; Inert atmosphere;
参考文献
Demir, Ayhan S.; Emrullahoglu, Mustafa; Pirkin, Eser; Akca, Nazmiye
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8992 - 8997