in neat (no solvent) byproducts: (CH2)5NH, CO2; under Ar; mixt. of carbamate and PhCH2OH (molar ratio 3.2:16) heated at 120°C (oil bath) for 1 h; isolated by vac. distn.; elem. anal.;
参考文献
Komarov; Ryzhkova; Andreev
Russian Chemical Bulletin, 2004 , vol. 53, # 4 p. 936 - 938
byproducts: H2O; dehydration of 1:2 mixt. of (C4H9)3SnOSn(C4H9)3 and alc.; separation of water formed by distillation or azeotropic distillation in benzene or toluene;
