1-(4-甲氧基苯基)-3,3-二(甲硫基)-2-丙烯-1-酮合成路线 (共 19 条)
反应条件
sodium ethanolate in ethanol Heating;
参考文献
Potts, Kevin T.; Cipullo, Michael J.; Ralli, Philip; Theodoridis, George
Journal of Organic Chemistry, 1982 , vol. 47, # 16 p. 3027 - 3038
反应条件
sodium 1.) THF, 2.) reflux, 1 d; Yield given. Multistep reaction;
参考文献
Huang, Zhi-Tang; Zhang, Ping-Cheng
Synthetic Communications, 1989 , vol. 19, # 17 p. 2999 - 3006
反应条件
9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran
3.5 h; Ambient temperature;
参考文献
Gammill, Ronald B.; Sobieray, Denis M.; Gold, Paul M.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3555 - 3558
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Arjona, Odon; Perez-Ossorio, Rafael; Perez-Rubalcaba, Alfredo; Quiroga, Maria L.; Romero, Dolores
Journal of Chemical Research, Miniprint, 1982 , # 9 p. 2351 - 2371
反应条件
CuCl2·2H2O
T=90°C; Knoevenagel cyclocondensation; 0.166667 h; Neat (no solvent);
参考文献
Singh, Okram Mukherjee; Devi, Nepram Sushuma; Devi, Laishram Ronibala; Lim, Ki Bum; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 175 - 178
反应条件
ammonium acetate; potassium tert-butylate
1.) THF, room temperature, 2.) glacial acetic acid; Yield given. Multistep reaction;
参考文献
Potts, Kevin T.; Cipullo, Michael J.; Ralli, Philip; Theodoridis, George
Journal of the American Chemical Society, 1981 , vol. 103, # 12 p. 3585 - 3586
反应条件
1: 100 percent / potassium tert-butoxide / tetrahydrofuran / 3 h / Ambient temperature
2: 48 percent / ammonium acetate / methanol / 3 h / Heating
View Scheme
参考文献
Potts, Kevin T.; Cipullo, Michael J.; Ralli, Philip; Theodoridis, George
Journal of Organic Chemistry, 1982 , vol. 47, # 16 p. 3027 - 3038
反应条件
hydrazine hydrate in methanol
4 h; Heating;
参考文献
Sunduru, Naresh; Agarwal, Anu; Katiyar, Sanjay Babu; Nishi; Goyal, Neena; Gupta, Suman; Chauhan, Prem M.S.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 23 p. 7706 - 7715
反应条件
1: 95 percent / NBS / CCl4 / 1.5 h / Ambient temperature
2: 54 percent / various solvent(s); pyridine / 1 h / 180 - 190 °C
View Scheme
参考文献
Singh, Gurdeep; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Synthesis, 1985 , # 2 p. 165 - 169