(S)-(+)-3,4,8,8a-四氢-8a-甲基-1,6-(2H,7H)-萘醌合成路线 （共 20 条）
反应条件
1: With aluminum oxide T=20°C; Michael addition; 0.166667 h; 2: With pyrrolidine Robinson annulation; 0.05 h; microwave irradiation;
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 4 p. 455 - 457
反应条件
pyridinium p-toluenesulfonate; (S)-pyrrolidine-2-carboxamide in acetonitrile T=50°C; Hajos-Parrish reaction; 144 h; enantioselective reaction;
参考文献
Synlett, , # 18 p. 2831 - 2835
反应条件
magnesium oxide T=100°C; Robinson annelation; P=75007.5 Torr; 2 h;
参考文献
Tetrahedron Letters, , vol. 45, # 26 p. 5147 - 5150
反应条件
boron trifluoride diethyl etherate in dichloromethane 1.) -78 deg C, 3 h, 2.) 25 deg C, 48 h;
参考文献
Journal of Organic Chemistry, , vol. 57, # 16 p. 4341 - 4342
反应条件
hydrogenchloride in ethanol T=80°C; 4.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1129 - 1134
反应条件
hydrogenchloride in ethanol T=80°C; 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1129 - 1134
反应条件
1: methanol. sodium methylate 2: oxalic acid; benzene View Scheme
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 300,309; engl. Ausg. S. 309, 315
反应条件
L-proline in N,N-dimethyl-formamide 168 h; Ambient temperature;
参考文献
Chemische Berichte, , vol. 118, # 11 p. 4330 - 4340
反应条件
1: trimethyl orthoformate, p-TsOH / 2 h 2: 55 percent / BF3*OEt2 / CH2Cl2 / 1.) -78 deg C, 3 h, 2.) 25 deg C, 2 days View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 2 p. 337 - 344
参考文献
Journal of the American Chemical Society, , vol. 82, p. 4039 - 4041
