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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
338945-22-5
合成路线
（共 33 条）
338945-22-5
→
反应条件
41720-98-3
(R)-(-)-2-甲基吡咯烷
反应条件
1: 86 percent / H2; Et3N / Pd/C / methanol / 20 °C 2: 96 percent / HCl gas / ethyl acetate / 2 h / 20 °C View Scheme
参考文献
Ku, Yi-Yin; Pu, Yu-Ming; Grieme, Tim; Sharma, Padam; Bhatia, Ashok V.; Cowart, Marlon
Tetrahedron, 2006 , vol. 62, # 18 p. 4584 - 4589
338945-22-5
→
反应条件
460746-46-7
(R)-4-(2-(2-(2-甲基吡咯烷-1-基)乙基)苯并呋喃-5-基)苯甲腈
反应条件
1: 86 percent / H2; Et3N / Pd/C / methanol / 20 °C 2: 96 percent / HCl gas / ethyl acetate / 2 h / 20 °C 3: K2CO3 / acetonitrile / 6 h / Heating 4: CuI; (i-Pr)2NH / PdCl2(PPh3)2 / acetonitrile / 20 °C View Scheme
参考文献
Ku, Yi-Yin; Pu, Yu-Ming; Grieme, Tim; Sharma, Padam; Bhatia, Ashok V.; Cowart, Marlon
Tetrahedron, 2006 , vol. 62, # 18 p. 4584 - 4589
338945-22-5
→
反应条件
41720-98-3
(R)-(-)-2-甲基吡咯烷
反应条件
1: 86 percent / H2; Et3N / Pd/C / methanol / 20 °C 2: 96 percent / HCl gas / ethyl acetate / 2 h / 20 °C View Scheme
参考文献
Ku, Yi-Yin; Pu, Yu-Ming; Grieme, Tim; Sharma, Padam; Bhatia, Ashok V.; Cowart, Marlon
Tetrahedron, 2006 , vol. 62, # 18 p. 4584 - 4589
338945-22-5
→
反应条件
157007-54-0
(R)-1-Boc-2-甲基吡咯烷
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol T=20°C;
参考文献
Ku, Yi-Yin; Pu, Yu-Ming; Grieme, Tim; Sharma, Padam; Bhatia, Ashok V.; Cowart, Marlon
Tetrahedron, 2006 , vol. 62, # 18 p. 4584 - 4589
338945-22-5
→
反应条件
202925-92-6
2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯
反应条件
n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Georgiou, Irene; Whiting, Andrew
European Journal of Organic Chemistry, 2012 , # 22 p. 4110 - 4113
1078-58-6
二苯锌
+
338945-22-5
→
反应条件
1194030-94-8
+
202925-92-6
2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯
反应条件
[Co(triphenylphosphane)2Cl2]; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=25°C; 1 h; Inert atmosphere;
参考文献
Hsu, Shih-Fan; Ko, Chih-Wei; Wu, Yao-Ting
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1756 - 1762
100-58-3
溴化苯基镁
+
338945-22-5
→
反应条件
1194030-94-8
+
202925-92-6
2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯
反应条件
[Co(triphenylphosphane)2Cl2]; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=25°C; 1 h; Inert atmosphere;
参考文献
Hsu, Shih-Fan; Ko, Chih-Wei; Wu, Yao-Ting
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1756 - 1762
5460-32-2
4-碘藜芦醚
+
338945-22-5
→
反应条件
反应条件
1: 4-iodoveratrole With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc in N,N-dimethyl-formamide T=0°C; Negishi coupling reaction; Inert atmosphere; 2: (S)-N-Boc-2-(iodomethyl)pyrrolidine in N,N-dimethyl-formamide T=0 - 20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
696-62-8
4-碘苯甲醚
+
338945-22-5
→
反应条件
1257984-85-2
+
202925-92-6
2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯
反应条件
1: para-iodoanisole With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc in N,N-dimethyl-formamide T=0°C; Negishi coupling reaction; Inert atmosphere; 2: (S)-N-Boc-2-(iodomethyl)pyrrolidine in N,N-dimethyl-formamide T=0 - 20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
401-81-0
3-碘三氟甲苯
+
338945-22-5
→
反应条件
1232830-21-5
+
202925-92-6
2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯
反应条件
1: 3-iodo-α,α,α-trifluorotoluene With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc in N,N-dimethyl-formamide T=0°C; Negishi coupling reaction; Inert atmosphere; 2: (S)-N-Boc-2-(iodomethyl)pyrrolidine in N,N-dimethyl-formamide T=0 - 20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
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