2-丙基-1,3-二氧戊环合成路线 （共 18 条）
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: US2012/330066 A1, 2012 ;
Location in patent: Page/Page column 11 ;
反应条件
hydrogen; 0.6 wt palladium on alumina T=210°C; P=16274.9 Torr; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: US2012/330068 A1, 2012 ;
Location in patent: Page/Page column 8 ;
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
反应条件
hydrogen; 0.6 wt palladium on alumina T=210°C; P=16274.9 Torr; Product distribution / selectivity;
参考文献
US2012/330066 A1, ;
Page/Page column 11 ;
参考文献
Bilger; Hibbert
Journal of the American Chemical Society, 1936 , vol. 58, p. 825
反应条件
γ-picolinium chlorochromate in dichloromethane T=20°C; 17 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 38, # 11 p. 1671 - 1673
反应条件
benzophenone; monofluoro-trichloromethane
Irradiation;
参考文献
Hartgerink,J.W. et al.
Tetrahedron, 1971 , vol. 27, p. 4323 - 4334
