3,5-二甲氧基-4-羟基苯基甲基甲醇合成路线 （共 10 条）
反应条件
in tetrahydrofuran T=0°C; 1 h; Inert atmosphere;
参考文献
Biannic, Berenger; Bozell, Joseph J.
Organic Letters, 2013 , vol. 15, # 11 p. 2730 - 2733
反应条件
1: C37H56CoN4O2; oxygen / methanol / 0 °C / |Inert atmosphere 2: tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere View Scheme
参考文献
Biannic, Berenger; Bozell, Joseph J.
Organic Letters, 2013 , vol. 15, # 11 p. 2730 - 2733
反应条件
sodium tetrahydroborate
参考文献
Takayama, Miyuki; Johjima, Toru; Yamanaka, Takeshi; Wariishi, Hiroyuki; Tanaka, Hiroo
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 1997 , vol. 53, # 10 p. 1621 - 1628
参考文献
Pospisek,J. et al.
Collection of Czechoslovak Chemical Communications, 1975 , vol. 40, p. 142 - 148
Full Text Show Details
Arlt et al.
Tappi, 1958 , vol. 41, p. 64,65
反应条件
hydrogenchloride; palladium on activated charcoal Hydrogenation;
参考文献
Arlt et al.
Tappi, 1958 , vol. 41, p. 64,65
反应条件
oxygen; (pyridine)lt;bis(salicylidene)ethylenediaminegt;cobalt in methanol P=2585.7 Torr; 24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2398 - 2404
反应条件
C44H60CoN4O2(2+); oxygen in methanol T=0°C; 16 h; Inert atmosphere;
参考文献
Biannic, Berenger; Bozell, Joseph J.
Organic Letters, 2013 , vol. 15, # 11 p. 2730 - 2733
反应条件
oxygen; (pyridine)lt;bis(salicylidene)ethylenediaminegt;cobalt in methanol P=2585.7 Torr; 24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2398 - 2404
反应条件
copper diacetate; ethylene glycol T=50°C; 8 h; Green chemistry; chemoselective reaction;
参考文献
Jiang, Jian-An; Chen, Cheng; Huang, Jian-Gang; Liu, Hong-Wei; Cao, Song; Ji, Ya-Fei
Green Chemistry, 2014 , vol. 16, # 3 p. 1248 - 1254
参考文献
Koutek,B. et al.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 2250 - 2255
