1-(4-氯苯基)乙醇合成路线 (共 156 条)
反应条件
in acetonitrile T=60°C; Kinetics;
参考文献
Lu, Yun; Bradshaw, Joshua; Zhao, Yu; Kuester, William; Kabotso, Daniel
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 12 p. 1172 - 1178
反应条件
in benzene Ambient temperatureIrradiationvarying concentration of initial compounds; Quantum yieldRate constant;
参考文献
Wagner, Peter J.; Zhang, Yuanda; Puchalski, Allen E.
Journal of Physical Chemistry, 1993 , vol. 97, p. 13368 - 13374
反应条件
Novozym 435; potassium tert-butylate; sodium carbonate; [2,3,4,5-Ph4(η5-C4CNH(i-Pr))]Ru(CO)2Cl in toluene T=25°C; 48 h;
参考文献
Choi, Jun Ho; Choi, Yoon Kyung; Kim, Yu Hwan; Park, Eun Sil; Kim, Eun Jung; Kim, Mahn-Joo; Park, Jaiwook
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1972 - 1977
反应条件
allyl alcohol in water T=30°C; 24 h; Geotrichum Candidum IFQ 5767;
参考文献
Nakamura, Kaoru; Inoue, Yuko; Matsuda, Tomoko; Ohno, Atsuyoshi
Tetrahedron Letters, 1995 , vol. 36, # 35 p. 6263 - 6266
反应条件
1: With (S)-(-)-3,3,5,5-tetramethyl-4H-dinaphtho[2,1-c:1',2'-e]-azipin-N-onyl in acetone 0.0833333 h; silica gel; 2: With sodium hydrogencarbonate; sodium bromide in water T=-15°C; 0.68 h; Electrolysis;
参考文献
EP1178026 A1, ;
Page 15 ;
反应条件
Arthrobacter atrocyaneus in N,N-dimethyl-formamide T=32°C; 72 h; Microbiological reaction; enantioselective reaction;
参考文献
Silva, Camila R.; Souza, Juliana C.; Araujo, Lidiane S.; Kagohara, Edna; Garcia, Thais P.; Pelizzari, Vivian H.; Andrade, Leandro H.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 83, p. 23 - 28
反应条件
in water 24 h; Geotrichum candidum IFO 5767, without and with allyl alcohol as an additive; Product distribution;
参考文献
Gong, Yinhan; Lee, Hian Kee
Analytical Chemistry, 2003 , vol. 75, # 6 p. 1348 - 1354
反应条件
polyoxyethylene (10) cetyl ether; n-octyl beta-D-glucopyranoside; subtilisin Carlsberg; sodium carbonate in tetrahydrofuran T=20°C; 15 h; Title compound not separated from byproducts;
参考文献
Boren, Linnea; Martin-Matute, Belen; Xu, Yongmei; Cordova, Armando; Baeckvall, Jan-E.
Chemistry - A European Journal, 2006 , vol. 12, # 1 p. 225 - 232
反应条件
[(C4Ph4COHOCC4Ph4)(μ-H)][(CO)4Ru2]; Novozym(R) 435; 2,4-dimethylpentan-3-one in toluene T=70°C; P=142.511 Torr; 40 h;
参考文献
Verzijl, Gerard K.M.; De Vries, Johannes G.; Broxterman, Quirinus B.
Tetrahedron Asymmetry, 2005 , vol. 16, # 9 p. 1603 - 1610
反应条件
Pseudomonas cepacia lipase in di-isopropyl ether T=30°C; Esterification; Racemate separation; 14 h;
参考文献
Athawale, Vilas; Manjrekar, Narendra
Synlett, 2000 , # 2 p. 225 - 226