1-(4-氯苯基)乙醇合成路线 （共 156 条）
反应条件
M. esculenta enzyme preparation immobilized on alginate gel in diethyl ether T=45°C; 116 h;
参考文献
Netto, Caterina G.C.M.; Andrade, Leandro H.; Toma, Henrique E.
Tetrahedron Asymmetry, 2009 , vol. 20, # 19 p. 2299 - 2304
反应条件
aluminium trichloride in hexane; toluene T=-5°C; 17 h; Title compound not separated from byproducts;
参考文献
Kashima, Choji; Mizuhara, Saori; Miwa, Yohei; Yokoyama, Yukihiro
Tetrahedron Asymmetry, 2002 , vol. 13, # 16 p. 1713 - 1719
反应条件
1: α-methyl-4-chlorobenzyl alcohol With (S,R(P))-2-phenyl-2,3-dihydroimidazo[1,2-a]pyrindinyl-pentaphenylcyclopentadienyliron; N-ethyl-N,N-diisopropylamine in toluene T=0°C; 0.0833333 h; 2: propionic acid anhydride in toluene T=0°C; 8 h; optical yield given as percent eeenantioselective reaction;
参考文献
Hu, Bin; Meng, Meng; Wang, Zheng; Du, Wenting; Fossey, John S.; Hu, Xinquan; Deng, Wei-Ping
Journal of the American Chemical Society, 2010 , vol. 132, # 47 p. 17041 - 17044
反应条件
steapsin lipase in hexane T=55°C; 48 h; Enzymatic reaction; optical yield given as percent ee;
参考文献
Dhake, Kishor P.; Deshmukh, Krishna M.; Wagh, Yogesh S.; Singhal, Rekha S.; Bhanage, Bhalchandra M.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 77, p. 15 - 23
反应条件
1: triethylamine / dichloromethane / 0 °C 2: Lipase Amano AK / 32 h / 20 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Bora, Pranjal P.; Bez, Ghanashyam; Anal, Jasha Momo H.
Journal of Molecular Catalysis B: Enzymatic, 2011 , vol. 72, # 3-4 p. 270 - 275
反应条件
1: dihydrogen peroxide; magnesium sulfate / 14 h / 0 - 20 °C 2: Raphanus sativus L. peroxidase; 2-methoxy-phenol / 7 h / 20 °C / pH 6 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Zilbeyaz, Kani; Kilic, Hamdullah; Sisecioglu, Melda; Ozdemir, Hasan; Guengoer, Azize Alayli
Tetrahedron Asymmetry, 2012 , vol. 23, # 8 p. 594 - 601
反应条件
iodosylbenzene in acetonitrile 1.5 h; Heating;
参考文献
Ueno, Makoto; Nabana, Takahiro; Togo, Hideo
Journal of Organic Chemistry, 2003 , vol. 68, # 16 p. 6424 - 6426
反应条件
in chloroform Heating;
参考文献
Abe; Sakuratani; Togo
Journal of Organic Chemistry, 2001 , vol. 66, # 18 p. 6174 - 6177
反应条件
0.0666667 h; microwave irradiation;
参考文献
Lee, Jong Chan; Lee, Ji Young; Lee, Seung Jun
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4939 - 4941
反应条件
1: m-chloroperbenzoic acid; KBr / iodobenzene / acetonitrile / 1 h / 20 °C 2: 88 percent / m-chloroperbenzoic acid / iodobenzene / acetonitrile / 5 h / 50 °C View Scheme
参考文献
Yamamoto, Yukiharu; Kawano, Yuhta; Toy, Patrick H.; Togo, Hideo
Tetrahedron, 2007 , vol. 63, # 22 p. 4680 - 4687
