1-(4-氯苯基)乙醇合成路线 (共 156 条)
反应条件
in acetone T=25°C; 3 h;
参考文献
Kovac, F.; Baumstark, A. L.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8751 - 8754
反应条件
(NH4)2S2O8; copper diacetate in acetic acid T=100°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Walling, Cheves; El-Taliawi, Gamil M.; Zhao, Chengxue
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4914 - 4917
反应条件
indium(III) chloride; diphenylchlorosilane in dichloromethane T=20°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 23 p. 7741 - 7744
反应条件
C42H36ClIrO2P2; potassium hydroxide in para-xylene T=130°C; 12 h; Inert atmosphereSchlenk techniqueMolecular sieve;
参考文献
Musa, Sanaa; Ackermann, Lutz; Gelman, Dmitri
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 3077 - 3080
反应条件
benzaldehyde; potassium hydroxide T=110°C; 32 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Xu, Qing; Chen, Jianhui; Liu, Quan
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 697 - 704
反应条件
Sodium bromate; sulfuric acid; sodium bromide in water T=60°C; 0.166667 h; Microwave irradiation;
参考文献
Paeaekkoenen, Sanna; Pursiainen, Jouni; Lajunen, Marja
Tetrahedron Letters, 2010 , vol. 51, # 51 p. 6695 - 6699
反应条件
para-chloroacetophenone; Al tri-t-BuO-; pyridinium bromide perbromide in toluene T=60°C; 24 h; Title compound not separated from byproducts;
参考文献
Cami-Kobeci, Gerta; Williams, Jonathan M.J.
Synlett, 2003 , # 1 p. 124 - 126
反应条件
Novozym 435; potassium tert-butylate; sodium carbonate; [2,3,4,5-Ph4(η5-C4CNH(i-Pr))]Ru(CO)2Cl in toluene T=25°C; 48 h;
参考文献
Choi, Jun Ho; Choi, Yoon Kyung; Kim, Yu Hwan; Park, Eun Sil; Kim, Eun Jung; Kim, Mahn-Joo; Park, Jaiwook
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1972 - 1977
反应条件
allyl alcohol in water T=30°C; 24 h; Geotrichum Candidum IFQ 5767;
参考文献
Nakamura, Kaoru; Inoue, Yuko; Matsuda, Tomoko; Ohno, Atsuyoshi
Tetrahedron Letters, 1995 , vol. 36, # 35 p. 6263 - 6266
反应条件
1: With (S)-(-)-3,3,5,5-tetramethyl-4H-dinaphtho[2,1-c:1',2'-e]-azipin-N-onyl in acetone 0.0833333 h; silica gel; 2: With sodium hydrogencarbonate; sodium bromide in water T=-15°C; 0.68 h; Electrolysis;
参考文献
EP1178026 A1, ;
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