1-(4-氯苯基)乙醇合成路线 (共 156 条)
反应条件
1: dihydrogen peroxide; magnesium sulfate / 14 h / 0 - 20 °C 2: Raphanus sativus L. peroxidase; 2-methoxy-phenol / 7 h / 20 °C / pH 6 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Zilbeyaz, Kani; Kilic, Hamdullah; Sisecioglu, Melda; Ozdemir, Hasan; Guengoer, Azize Alayli
Tetrahedron Asymmetry, 2012 , vol. 23, # 8 p. 594 - 601
反应条件
tricarbonyl(tetraphenylcyclopentadienone)iron; N,N,N-triethylamine N-oxide in acetone T=60°C; 6 h; Inert atmosphere;
参考文献
Johnson, Tarn C.; Clarkson, Guy J.; Wills, Martin
Organometallics, 2011 , vol. 30, # 7 p. 1859 - 1868
反应条件
silver(l) oxide; (η5-Ph5C5)Ru(CO)(PPh3)Br in toluene T=50°C; 2 h;
参考文献
Ko, Soo-Byung; Baburaj, Baskar; Kim, Mahn-Joo; Park, Jaiwook
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6860 - 6864
反应条件
Re2O7 in toluene T=100°C; 24 h;
参考文献
Korstanje, Ties J.; Jastrzebski, Johann T. B. H.; Gebbink, Robertus J. M. Klein
ChemSusChem, 2010 , vol. 3, # 6 p. 695 - 697
反应条件
sodium azide; iodine; sodium hydrogencarbonate in water T=100 - 105°C;
参考文献
Rajendar; Kant, Ruchir; Narender
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3591 - 3596
反应条件
1: MnO2 / CH2Cl2 2: I2 / 14 h / 100 °C View Scheme
参考文献
Wipf, Peter; Aslan, Diana C.; Southwick, Eileen C.; Lazo, John S.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 3 p. 313 - 317
反应条件
potassium hydroxide; hydrogen; Aliquatreg; 336; platinum on activated charcoal in 2,2,4-trimethylpentane T=50°C; 7 h;
参考文献
Selva, Maurizio; Tundo, Pietro; Perosa, Alvise
Journal of Organic Chemistry, 1998 , vol. 63, # 10 p. 3266 - 3271
反应条件
potassium hydroxide T=135°C; 8 h; Inert atmosphereSchlenk technique;
参考文献
Xu, Qing; Chen, Jianhui; Liu, Quan
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 697 - 704
反应条件
in benzene Ambient temperatureIrradiationvarying concentration of initial compounds; Quantum yieldRate constant;
参考文献
Wagner, Peter J.; Zhang, Yuanda; Puchalski, Allen E.
Journal of Physical Chemistry, 1993 , vol. 97, p. 13368 - 13374
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in various solvent(s)
T=180°C; 3 h; Product distribution;
参考文献
Pri-Bar, Ilan; Buchman, Ouri; Schumann, Hebert; Kroth, Heinz J.; Blum, Jochanan
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4418 - 4428