1-(4-氯苯基)乙醇合成路线 （共 156 条）
反应条件
N,N-dichloro-2-methyl-2-propanamine in tetrachloromethane
T=20°C; 1 h; Irradiation; Product distribution;
参考文献
Ogata, Yoshiro; Kimura, Makoto
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 947 - 950
反应条件
tris(pentafluorophenyl)-borane in acetonitrile
T=20°C; 1 h;
参考文献
Rajagopal, Gurusamy; Kim, Sung Soo
Tetrahedron, 2009 , vol. 65, # 22 p. 4351 - 4355
反应条件
1: SOCl2 / Heating
2: NH3 / tetrahydrofuran / 1 h / 0 - 20 °C
View Scheme
参考文献
Aramini, Andrea; Cesta, Maria C.; Coniglio, Silvia; Bijani, Christian; Colagioia, Sandro; D'Elia, Valerio; Allegretti, Marcello
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7911 - 7914
反应条件
potassium hydroxide in toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Wang, Dong; Guo, Xu-Qing; Wang, Chen-Xi; Wang, Ya-Nong; Zhong, Rui; Zhu, Xiao-Han; Cai, Li-Hua; Gao, Zi-Wei; Hou, Xiu-Feng
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1117 - 1125
反应条件
benzaldehyde; potassium hydroxide
T=110°C; 32 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Xu, Qing; Chen, Jianhui; Liu, Quan
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 697 - 704
反应条件
sodium hydroxide; [{(η5-C5Me5)IrCl}2(μ-Cl)2] in toluene
T=110°C; 17 h;
参考文献
Fujita, Ken-Ichi; Asai, Chiho; Yamaguchi, Tetsuhiro; Hanasaka, Fumihiro; Yamaguchi, Ryohei
Organic Letters, 2005 , vol. 7, # 18 p. 4017 - 4019
反应条件
C42H36ClIrO2P2; potassium hydroxide in para-xylene
T=130°C; 12 h; Inert atmosphereSchlenk techniqueMolecular sieve;
参考文献
Musa, Sanaa; Ackermann, Lutz; Gelman, Dmitri
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 3077 - 3080
反应条件
sodium hydrogen sulphate; silica gel in 1,2-dichloro-ethane
T=60°C; 4 h;
参考文献
Aoyama, Tadashi; Koda, Shuichi; Takeyoshi, Yuka; Ito, Tetsuhiro; Takido, Toshio; Kodomari, Mitsuo
Chemical Communications, 2013 , vol. 49, # 59 p. 6605 - 6607
反应条件
in chloroform-d1
T=35°C; MechanismRate constant;
参考文献
Gillen, Ciaran J.; Knipe, Anthony C.; Watts, William E.
Tetrahedron Letters, 1981 , vol. 22, p. 597 - 600
反应条件
1: PBr3, Py / diethyl ether
2: NaOEt / ethanol
3: (i) aq. KOH, EtOH, (ii) (decarboxylation)
View Scheme
参考文献
Kuchar; Brunova; Rejholec; et al.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, # 2 p. 633 - 646
