1-(4-氯苯基)乙醇合成路线 (共 156 条)
反应条件
dioxomolybdenum(VI)-dichloro[4,4'-dicarbixylato-2,2'-bipyridine]-anchored TiO2 in acetonitrile T=3 - 20°C; P=912.061 Torr; 7 h; Inert atmosphereUV-irradiation;
参考文献
Transition Metal Chemistry, , vol. 36, # 8 p. 897 - 900
反应条件
water; hydrogen; Aliquatreg; 336; platinum on activated charcoal in 2,2,4-trimethylpentane T=50°C; P=760 Torr; KineticsProduct distribution; Further Variations:pH-valuesReagents;
参考文献
Journal of Catalysis, , vol. 196, # 2 p. 330 - 338
反应条件
(1R,2S)-(+)-2-dibutylamino-1-phenyl-1-propanol in tetrahydrofuran; toluene T=20°C; 16 h; Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 38 p. 3945 - 3947
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: water; dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; hexane / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 14, # 9 p. 2262 - 2265
反应条件
1.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere 2.1: potassium hydrogen persulfate / methanol; water / 12 h / 0 - 20 °C / Inert atmosphere 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere 3.2: 0 - 20 °C / Inert atmosphere 4.1: water; dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; hexane / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 14, # 9 p. 2262 - 2265
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1295,1297
Zhurnal Obshchei Khimii, , vol. 14, p. 120,123
Chem.Abstr., , p. 916
Organic Syntheses, , vol. Coll. Vol. III, p. 200
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 10 p. 1737 - 1740
参考文献
Journal of the American Chemical Society, , vol. 65, p. 2054,2056
Journal of the Chemical Society, , p. 203,205
反应条件
(tin(IV) ethoxide)(n) in toluene T=110°C; 20 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 407 - 411
反应条件
sodium tetrahydroborate; β-cyclodextrin in water T=20°C; 67 h;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 2 p. 161 - 166