1-(4-氯苯基)乙醇合成路线 (共 156 条)
反应条件
1: pyridine / 2 h / Cooling with ice 2: water; N,N-dimethyl-aniline / acetonitrile / 25 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 11 p. 4652 - 4660
反应条件
1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 1 h / Reflux 2: pyridine / 2 h / Cooling with ice 3: water; N,N-dimethyl-aniline / acetonitrile / 25 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 11 p. 4652 - 4660
反应条件
1: bis(2-((2,6-diisopropylphenyl)iminomethyl)phenoxide)nickel(II); (pentamethylcyclopentadienyl)IrCl2(1-benzyl-3-methylimidazol-2-ylidene); potassium tert-butylate / isopropyl alcohol / 24 h / 80 °C / Inert atmosphere 2: C68H88Cl4Ir2N6NiO2; potassium tert-butylate / isopropyl alcohol / 24 h / 80 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 39 p. 11041 - 11051
反应条件
sodium tetrahydroborate; tin(ll) chloride in tetrahydrofuran 1.5 h; Heatingselectivity, absence of SnCl2, further solvents;
参考文献
Chemistry Letters, , p. 853 - 854
参考文献
Journal of Organic Chemistry, , vol. 23, p. 935
反应条件
(+/-)-3-exo-(dimethylamino)isoborneol in toluene T=40°C; Product distributionRate constant;
参考文献
Tetrahedron, , vol. 55, # 12 p. 3605 - 3614
反应条件
potassium tert-butylate; palladium dichloride; α,α'-bis(di-t-butylphosphino)-o-xylene T=100°C; 48 h;
参考文献
Dalton Transactions, , # 10 p. 1826 - 1830
反应条件
water in acetone T=55 - 80°C; Kinetics;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 48, # 11 p. 3337 - 3346
反应条件
potassium tert-butylate; palladium dichloride; α,α'-bis(di-t-butylphosphino)-o-xylene T=100°C; 48 h; Further byproducts given;
参考文献
Dalton Transactions, , # 10 p. 1826 - 1830
反应条件
in hydrogenchloride; ethanol; butan-1-ol Ambient temperaturecathode: Pb plate (ca. 21.3 cm2); Pt plate (ca. 4.0 cm2), constant current density (-3.7 mA/cm2);
参考文献
Chemistry Letters, , # 9 p. 1719 - 1720