1-(4-氯苯基)乙醇合成路线 (共 156 条)
反应条件
1-benzyl-1-aza-4-azoniabicyclolt;2.2.2gt;octane periodate in acetonitrile 15 h; Heating;
参考文献
Hajipour, Abdol Reza; Baltork, Iraj Mohammadpoor; Kianfar, Godaraz
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 11 p. 2655 - 2659
反应条件
Arthrobacter atrocyaneus in N,N-dimethyl-formamide T=32°C; 48 h; Microbiological reaction; enantioselective reaction;
参考文献
Silva, Camila R.; Souza, Juliana C.; Araujo, Lidiane S.; Kagohara, Edna; Garcia, Thais P.; Pelizzari, Vivian H.; Andrade, Leandro H.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 83, p. 23 - 28
反应条件
1: With (S)-(-)-3,3,5,5-tetramethyl-4H-dinaphtho[2,1-c:1',2'-e]-azipin-N-onyl in acetone 0.0833333 h; silica gel; 2: With sodium hydrogencarbonate; sodium bromide in water T=-15°C; 0.68 h; Electrolysis;
参考文献
EP1178026 A1, ;
Page 15 ;
反应条件
Arthrobacter atrocyaneus in N,N-dimethyl-formamide T=32°C; 72 h; Microbiological reaction; enantioselective reaction;
参考文献
Silva, Camila R.; Souza, Juliana C.; Araujo, Lidiane S.; Kagohara, Edna; Garcia, Thais P.; Pelizzari, Vivian H.; Andrade, Leandro H.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 83, p. 23 - 28
反应条件
potassium hydroxide; acetone; N,N'-bis[o-(diphenylphosphino)benzylidene]-1R,2R-diaminocyclohexane; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in isopropyl alcohol T=25°C; 5 h;
参考文献
Li, Yan-Yun; Zhang, Xue-Qin; Dong, Zhen-Rong; Shen, Wei-Yi; Chen, Gui; Gao, Jing-Xing
Organic Letters, 2006 , vol. 8, # 24 p. 5565 - 5567
反应条件
oxygen in 1,2-dichloro-ethane T=20°C;
参考文献
Bai, Xing-Feng; Gao, Guang; Zheng, Zhan-Jiang; Li, Fei; Lai, Guo-Qiao; Jiang, Kezhi; Li, Fuwei; Xu, Li-Wen
Synlett, 2011 , # 20 art. no. W20211ST, p. 3031 - 3035
反应条件
(NH4)2S2O8; copper diacetate in acetic acid T=100°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Walling, Cheves; El-Taliawi, Gamil M.; Zhao, Chengxue
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4914 - 4917
反应条件
[(C4Ph4COHOCC4Ph4)(μ-H)][(CO)4Ru2]; Novozym(R) 435; 2,4-dimethylpentan-3-one in toluene T=70°C; P=142.511 Torr; 40 h;
参考文献
Verzijl, Gerard K.M.; De Vries, Johannes G.; Broxterman, Quirinus B.
Tetrahedron Asymmetry, 2005 , vol. 16, # 9 p. 1603 - 1610
反应条件
Sodium bromate; sulfuric acid; sodium bromide in water T=60°C; 0.166667 h; Microwave irradiation;
参考文献
Paeaekkoenen, Sanna; Pursiainen, Jouni; Lajunen, Marja
Tetrahedron Letters, 2010 , vol. 51, # 51 p. 6695 - 6699
反应条件
bacteria HK1D10 in N,N-dimethyl-formamide T=20°C; pH=7; 72 h; Microbiological reactionaq. phosphate buffer; enantioselective reaction;
参考文献
Araujo, Lidiane S.; Kagohara, Edna; Garcia, Thais P.; Pellizari, Vivian H.; Andrade, Leandro H.
Marine Drugs, 2011 , vol. 9, # 5 p. 889 - 905