1-(4-氯苯基)乙醇合成路线 (共 156 条)
反应条件
para-chloroacetophenone; Al tri-t-BuO-; pyridinium bromide perbromide in toluene T=60°C; 24 h; Title compound not separated from byproducts;
参考文献
Cami-Kobeci, Gerta; Williams, Jonathan M.J.
Synlett, 2003 , # 1 p. 124 - 126
反应条件
tricarbonyl(tetraphenylcyclopentadienone)iron; N,N,N-triethylamine N-oxide in toluene T=60°C; 3 h; Inert atmosphere;
参考文献
Johnson, Tarn C.; Clarkson, Guy J.; Wills, Martin
Organometallics, 2011 , vol. 30, # 7 p. 1859 - 1868
反应条件
N,N-dichloro-2-methyl-2-propanamine in tetrachloromethane T=20°C; 1 h; Irradiation; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 947 - 950
反应条件
tricarbonyl(tetraphenylcyclopentadienone)iron; N,N,N-triethylamine N-oxide in acetone T=60°C; 6 h; Inert atmosphere;
参考文献
Johnson, Tarn C.; Clarkson, Guy J.; Wills, Martin
Organometallics, 2011 , vol. 30, # 7 p. 1859 - 1868
反应条件
in acetone T=25°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 35, # 47 p. 8751 - 8754
反应条件
lt;Mn3O(OAc)6(OAc)(HOAc)gt;*5H2O; lithium chloride in acetic acid 0.3 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 11 p. 3567 - 3571
反应条件
lt;Mn3O(OAc)6(OAc)(HOAc)gt;*5H2O; lithium chloride in acetic acid 0.3 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 11 p. 3567 - 3571
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C 2: iodine / neat (no solvent) / 2 h / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in various solvent(s) T=180°C; 3 h; Product distribution;
参考文献
Pri-Bar, Ilan; Buchman, Ouri; Schumann, Hebert; Kroth, Heinz J.; Blum, Jochanan
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4418 - 4428
反应条件
potassium hydroxide T=135°C; 8 h; Inert atmosphereSchlenk technique;
参考文献
Xu, Qing; Chen, Jianhui; Liu, Quan
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 697 - 704