1,1'-硫代二-1-丙烯合成路线 （共 16 条）
反应条件
potassium hydroxide; dimethyl sulfoxide T=90°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Musorin, G. K.; Krivdin, L. B.; Amosova, S. V.; Kalabin, G. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 9 p. 1806 - 1807
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 9 p. 2004 - 2005
反应条件
(i) HCl, H2S, (ii) PhNEt2; Multistep reaction;
参考文献
Brandsma,L.; Arens,J.F.
Recueil des Travaux Chimiques des Pays-Bas, 1962 , vol. 81, p. 33 - 38
参考文献
Tarbell; Lovett
Journal of the American Chemical Society, 1956 , vol. 78, p. 2259,2262
反应条件
T=500 - 520°C; pyrolysis at atmospheric pressure in a nitrogen stream; Further byproducts given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , p. 466
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 24, # 4 p. 561
反应条件
T=560 - 580°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Ostroukhova, L. A.; Deryagina, E. N.; Korchevin, N. A.; Musorin, G. K.; Amosova, S. V.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 2.2 p. 301 - 305
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 2 p. 354 - 359
反应条件
T=420°C; Product distribution; Further Variations:Temperatures;
参考文献
Deryagina; Sukhomazova; Levanova; Shilkina; Korchevin
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 3 p. 359 - 363
反应条件
T=520°C; reaction in the presence of dimethyl selenide, 2-halothiophenes and acetylene, var. temp.; Product distributionMechanism;
参考文献
Ostroukhova, L. A.; Deryagina, E. N.; Korchevin, N. A.; Musorin, G. K.; Amosova, S. V.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 2.2 p. 301 - 305
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 2 p. 354 - 359
反应条件
hydrogen fluoride T=14 - 16°C; 122 h; Electrochemical reaction; Product distribution;
参考文献
Grigor'eva; Shainyan; Kaurova; Gracheva; Lesnevskaya; Barabanov
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 7 p. 1095 - 1100
反应条件
T=500 - 520°C; pyrolysis at atmospheric pressure in a nitrogen stream; Further byproducts given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , p. 466
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 24, # 4 p. 561
反应条件
T=520°C; reaction in the presence of dimethyl selenide, 2-halothiophenes and acetylene, var. temp.; Product distributionMechanism;
参考文献
Ostroukhova, L. A.; Deryagina, E. N.; Korchevin, N. A.; Musorin, G. K.; Amosova, S. V.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 2.2 p. 301 - 305
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 2 p. 354 - 359
