4,4’-二甲氧基二苯硫醚合成路线 （共 41 条）
反应条件
potassium phosphate; copper(l) iodide; potassium thioacyanate in PEG-400 T=150°C; 20 h; Inert atmosphere;
参考文献
Chen, Junmin; Zhang, Yimin; Liu, Li; Yuan, Tangjun; Yi, Fei
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1284 - 1290
反应条件
potassium phosphate; copper(l) iodide; Na2S*9H2O T=150°C; 24 h;
参考文献
Chen, Junmin; Zhang, Yimin; Liu, Li; Yuan, Tangjun; Yi, Fei
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1284 - 1290
反应条件
thionyl chloride; triphenylphosphine in tetrahydrofuran T=20°C; 4 h; Inert atmosphere;
参考文献
Jang, Yujin; Kim, Kyoung Tae; Jeon, Heung Bae
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 6328 - 6331
反应条件
CyPF-tBu; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether T=110°C; 2 h; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1664 - 1672
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; bis[2-(diphenylphosphino)phenyl] ether in toluene T=100°C; 2 h;
参考文献
Bagley, Mark C.; Fusillo, Vincenzo; Hills, Edward G.B.; Mulholland, Alex T.; Newcombe, Joseph; Pentecost, Leanne J.; Radley, Emily L.; Stephens, Bethan R.; Turrell, Christopher C.
Arkivoc, 2012 , vol. 2012, # 7 p. 294 - 313
反应条件
potassium tert-butylate; palladium diacetate; Josiphos SL-J009-1 in toluene T=110°C; 6 - 12 h; Product distribution / selectivity;
参考文献
YALE UNIVERSITY
Patent: WO2007/64869 A2, 2007 ;
Location in patent: Page/Page column 17-18 ;
反应条件
potassium tert-butylate; CyPF-t-Bu; bis(dibenzylideneacetone)-palladium(0) in toluene T=110°C;
参考文献
Fernandez-Rodriguez, Manuel A.; Shen, Qilong; Hartwig, John F.
Chemistry - A European Journal, 2006 , vol. 12, # 30 p. 7782 - 7796
反应条件
1: With copper(l) iodide; K2S in N,N-dimethyl-formamide T=80°C; 12 h; Inert atmosphere; 2: With hydrogenchloride; triphenylphosphine in 1,4-dioxane; water; N,N-dimethyl-formamide T=40°C; 5 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 22 p. 5250 - 5253
反应条件
morpholinesulfenyl chloride; boron trifluoride in dichloromethane T=-78 - 25°C;
参考文献
Bombala, Mboro U.; Ley, Steven V.
Synthetic Communications, 1980 , vol. 10, # 4 p. 291 - 298
反应条件
antimony(V) pentachloride in dichloromethane T=25°C; 2 h;
参考文献
Takeuchi, Hiroshi; Hiyama, Takehiro; Kamai, Noriyoshi; Oya, Hiromi
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 11 p. 2301 - 2305
