4,4’-二甲氧基二苯硫醚合成路线 (共 41 条)
反应条件
carbon disulfide; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene T=100°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 10 p. 5001 - 5006
反应条件
1: (4-methoxyphenyl)-boronic acid With potassium ethylxanthate; copper(l) chloride in methanol 3 h; Inert atmosphereReflux; 2: (4-methoxyphenyl)-boronic acid With potassium hydroxide in methanol 5 h; Inert atmosphereReflux;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Synlett, 2011 , # 20 art. no. W18411ST, p. 3041 - 3045
反应条件
4-MeC6H4SNa in N,N-dimethyl-formamide T=26°C; 44 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 26, # 6 p. 775 - 778
反应条件
1-phenyl-2,2,2-trifluorodiazoethane; oxygen; 5,15,10,20-tetraphenylporphyrin in dichloromethane; acetonitrile T=20°C; 0.5 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 28, # 49 p. 6201 - 6204
反应条件
sulfur; copper(l) iodide; lithium hydroxide hydrate in N,N-dimethyl-formamide T=100°C; 168 h; Inert atmosphere;
参考文献
Organometallics, , vol. 32, # 19 p. 5514 - 5522
反应条件
in acetic acid T=120 - 125°C; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1957 - 1960
反应条件
1: 1-bromo-4-methoxy-benzene With potassium tert-butylate; thiourea in dimethyl sulfoxide 3 h; UV-irradiation; 2: methyl iodide in water; dimethyl sulfoxide Title compound not separated from byproducts;
参考文献
Organic Letters, , vol. 5, # 22 p. 4133 - 4136
反应条件
1: para-iodoanisole With potassium tert-butylate; thiourea in dimethyl sulfoxide 3 h; UV-irradiation; 2: methyl iodide in water; dimethyl sulfoxide Title compound not separated from byproducts;
参考文献
Organic Letters, , vol. 5, # 22 p. 4133 - 4136
参考文献
Justus Liebigs Annalen der Chemie, , vol. 576, p. 35,60
参考文献
Journal of Fluorine Chemistry, , vol. 19, p. 91 - 96