4,4’-二甲氧基二苯硫醚合成路线 （共 41 条）
反应条件
1: para-iodoanisole With potassium tert-butylate; thiolacetic acid potassium salt in dimethyl sulfoxide 3 h; Irradiation; 2: methyl iodide in water; dimethyl sulfoxide
参考文献
European Journal of Organic Chemistry, , # 9 p. 2210 - 2214
反应条件
1: 2-methyl-propan-2-ol; H2O / 5.5 h / 20 - 25 °C / Irradiation; DRL-400 mercury lamp (400 W) 2: KOH / H2O / 0.33 h / Heating 3: air / H2O / 3 h / Ambient temperature 4: triphenylphosphine / benzene / 10 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
1: air / H2O / 3 h / Ambient temperature 2: triphenylphosphine / benzene / 10 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
1: 86 percent / sodium sulphite / H2O 2: thionyl chloride / CHCl3 / Ambient temperature 3: pyridine / CHCl3 / 1 h / 5 - 10 °C 4: 32 percent / acetic acid / 120 - 125 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1957 - 1960
参考文献
Chemische Berichte, , vol. 73, p. 145,152
反应条件
in tetrachloromethane Ambient temperature;
参考文献
Tetrahedron, , vol. 37, # 18 p. 3115 - 3120
反应条件
thionyl chloride; zinc(II) chloride in 1,2-dichloro-ethane T=0 - 2°C; 2 h; other Friedel-Crafts catalysts, other solvents; Product distribution;
参考文献
Australian Journal of Chemistry, , vol. 38, # 8 p. 1209 - 1221
反应条件
bismuth Oxychloride; thionyl chloride T=60°C; 1 h; Product distribution; Further Variations:ReagentsTemperaturesreaction time;
参考文献
Synlett, , # 5 p. 631 - 634
反应条件
Kinetics; byproducts: HCl; at 500-600°C;
参考文献
Phosphorus Sulfur, , vol. 7, p. 123 - 132
S: SVol.4a/b, 1.3.11.7, page 302 - 302
Top. Org. Sulphur Chem. Plenary Lect. 8th Intern. Symp., Portoroz, Yugosl., 1978, pp. 363/87
反应条件
in acetic acid T=120 - 125°C; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1957 - 1960
