3-硝基苯甲醛二甲基乙缩醛合成路线 （共 18 条）
反应条件
(i) MeOH, (ii) Et3N, benzene; Multistep reaction;
参考文献
Kantlehner,W. et al.
Liebigs Annalen der Chemie, 1979 , p. 522 - 527
反应条件
water; acetone; mesoporous aluminosilicate T=55°C; 2 h;
参考文献
Robinson, Mathew W.C.; Graham, Andrew E.
Tetrahedron Letters, 2007 , vol. 48, # 27 p. 4727 - 4731
反应条件
sodium hydroxide in water
参考文献
Bayer Aktiengesellschaft
Patent: US4910345 A1, 1990 ;
参考文献
Bayer Aktiengesellschaft
Patent: US4910345 A1, 1990 ;
反应条件
T=80 - 130°C; P=88260.9 Torr; Hydrogenation;
参考文献
Eastman-Kodak Co.
Patent: US2382613 , 1943 ;
反应条件
1: 87 percent / Na2S*9H2O; hydrochloric acid / H2O / 8 h / Heating 2: sodium carbonate / diethyl ether / 96 h / 20 °C 3: sulfuric acid / H2O / 1 h / Heating View Scheme
参考文献
Rodriguez, J. Gonzalo; Lafuente, Antonio; Martin-Villamil, Rosa; Martinez-Alcazar, M. Paz
Journal of Physical Organic Chemistry, 2001 , vol. 14, # 12 p. 859 - 868
反应条件
triethylsilane; iodine in acetonitrile 5 h; Inert atmosphereReflux; chemoselective reaction;
参考文献
Zhang, Xue-Lin; Yu, Pan; Wu, Yong-Wei; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2014 , vol. 38, # 5 p. 261 - 264
反应条件
hydrogenchloride; sodium sulfide in water
8 h; Heating;
参考文献
Rodriguez, J. Gonzalo; Lafuente, Antonio; Martin-Villamil, Rosa; Martinez-Alcazar, M. Paz
Journal of Physical Organic Chemistry, 2001 , vol. 14, # 12 p. 859 - 868
