1-(二甲氧基甲基)-4-甲基苯合成路线 （共 28 条）
反应条件
sodium tetrafluoroborate; sulfuric acid 1.) anodic oxidation, AcOH, MeOH, 2.) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nishiguchi, Ikuzo; Hirashima, Tsuneaki
Journal of Organic Chemistry, 1985 , vol. 50, # 4 p. 539 - 541
反应条件
triethylsilane; acetyl chloride; tin(ll) chloride in dichloromethane 3 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Tsukamoto, Kazuhisa; Ichimura, Yuichi; Koga, Gen
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1410 - 1412
反应条件
1: dichloromethane / 0.5 h / 0 °C 2: oxygen / dichloromethane / 0 °C View Scheme
参考文献
Goto, Akihiro; Otake, Kazuki; Kubo, Ozora; Sawama, Yoshinari; Maegawa, Tomohiro; Fujioka, Hiromichi
Chemistry - A European Journal, 2012 , vol. 18, # 36 p. 11423 - 11432
反应条件
ammonium chloride; β-cyclodextrin; zinc in water T=50°C; Barbier-type allylation reaction; 8 h;
参考文献
Surendra; Krishnaveni, N. Srilakshmi; Rao, K. Rama
Tetrahedron Letters, 2006 , vol. 47, # 13 p. 2133 - 2136
反应条件
MoVIO2(acetylacetone)2 in acetonitrile 4 h;
参考文献
Synthetic Communications, , vol. 25, # 17 p. 2529 - 2532
反应条件
PMES-SO3H-NH2-B T=90°C; Henry reaction; 24 h;
参考文献
Chemical Communications, , vol. 47, # 37 p. 10422 - 10424
反应条件
MS-SO3H(at)MS(at)MS-NH2 in toluene
T=80°C; 0.5 h; Reagent/catalyst;
参考文献
Li, Ping; Cao, Chang-Yan; Liu, Hua; Yu, Yu; Song, Wei-Guo
Journal of Materials Chemistry A, 2013 , vol. 1, # 41 p. 12804 - 12810
反应条件
triethylsilane; iodine in acetonitrile
T=20°C; 5 h; Inert atmosphere; chemoselective reaction;
参考文献
Zhang, Xue-Lin; Yu, Pan; Wu, Yong-Wei; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2014 , vol. 38, # 5 p. 261 - 264
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide
T=65°C; 4 h;
参考文献
Jensen, Henrik Helligso; Nordstrom, Lars Ulrik; Bols, Mikael
Journal of the American Chemical Society, 2004 , vol. 126, # 30 p. 9205 - 9213
反应条件
in liquid sulphur dioxide
T=-60°C; 72 h;
参考文献
Mayr, Herbert; Gorath, Gorden; Bauer, Bernhard
Angewandte Chemie, 1994 , vol. 106, # 7 p. 793 - 794
