2-甲基-DL-丝氨酸水合物合成路线 （共 21 条）
反应条件
ammonia; lithium in tetrahydrofuran; tert-butyl alcohol T=-78°C; 0.166667 h;
参考文献
Colson, Pierre-Jean; Hegedus, Louis S.
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 5918 - 5924
反应条件
hydrogenchloride in tetrahydrofuran T=90°C; 4 h;
参考文献
Wang, Hai-Fei; Ma, Guo-Hua; Yang, Shao-Bo; Han, Rong-Gang; Xu, Peng-Fei
Tetrahedron Asymmetry, 2008 , vol. 19, # 13 p. 1630 - 1635
反应条件
hydrogenchloride T=120°C; 1.5 h; freeing from salt with Dowex W50*X8;
参考文献
Seebach, Dieter; Aebi, Johannes D.
Tetrahedron Letters, 1984 , vol. 25, # 24 p. 2545 - 2548
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 24 h;
参考文献
Avenoza, Alberto; Cativiela, Carlos; Corzana, Francisco; Peregrina, Jesus M.; Sucunza, David; Zurbano, Maria M.
Tetrahedron Asymmetry, 2001 , vol. 12, # 6 p. 949 - 957
反应条件
hydrogenchloride T=90°C; 6 h;
参考文献
Wang, Hai-Fei; Ma, Guo-Hua; Yang, Shao-Bo; Han, Rong-Gang; Xu, Peng-Fei
Tetrahedron Asymmetry, 2008 , vol. 19, # 13 p. 1630 - 1635
反应条件
hydrogen; palladium on activated charcoal in methanol 48 h; Ambient temperature;
参考文献
Carda; Murga; Rodriguez; Gonzalez; Castillo; Marco
Tetrahedron Asymmetry, 1998 , vol. 9, # 10 p. 1703 - 1712
反应条件
methyloxirane in ethanol 2 h; Heating;
参考文献
Aydillo, Carlos; Jimenez-Oses, Gonzalo; Busto, Jesus H.; Peregrina, Jesus M.; Zurbano, Maria M.; Avenoza, Alberto
Chemistry - A European Journal, 2007 , vol. 13, # 17 p. 4840 - 4848
反应条件
potassium hydroxide; potassium phosphate buffer; porcine kidney acylase I T=40°C; relative initial rate of hydrolysis, also without CoCl2;
参考文献
Chenault, H. Keith; Dahmer, Juergen; Whitesides, George M.
Journal of the American Chemical Society, 1989 , vol. 111, # 16 p. 6354 - 6364
反应条件
potassium hydroxide; potassium phosphate buffer; porcine kidney acylase I T=40°C; relative initial rate of hydrolysis;
参考文献
Chenault, H. Keith; Dahmer, Juergen; Whitesides, George M.
Journal of the American Chemical Society, 1989 , vol. 111, # 16 p. 6354 - 6364
反应条件
hydrogenchloride T=80°C; 6 h; Yield given;
参考文献
Ito, Yoshihiko; Sawamura, Masaya; Shirakawa, Eiji; Hayashizaki, Keiichi; Hayashi, Tamio
Tetrahedron Letters, 1988 , vol. 29, # 2 p. 235 - 238
