N-邻苯二甲酰-L-谷氨酸合成路线 (共 20 条)
反应条件
1: With sodium carbonate in water T=20°C; 5.25 h; 2: With hydrogenchloride in water pH=1 - 2; 2 h;
参考文献
US2008/26017 A1, ;
Page/Page column 6 ;
反应条件
acetic acid T=145°C; 1 h;
参考文献
Biomacromolecules, , vol. 12, # 7 p. 2466 - 2474
反应条件
sodium carbonate in water T=0 - 20°C; 0.75 h; Inert atmosphere;
参考文献
Organic Process Research and Development, , vol. 9, # 6 p. 853 - 856
反应条件
hydrogenchloride in acetic acid 2 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 53, # 6 p. 1167 - 1170
反应条件
N-ethyl-N,N-diisopropylamine in water; acetonitrile 0.166667 h; Ambient temperature;
参考文献
Synthesis, , # 10 p. 1419 - 1420
参考文献
Journal of Biological Chemistry, , vol. 207, p. 477,485
Journal of the Chemical Society, , p. 873,879
参考文献
Journal of the American Chemical Society, , vol. 77, p. 2843
反应条件
1: 78 percent / 0.25 h / Ambient temperature 2: 77 percent / (i-Pr)2NEt / acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 10 p. 1419 - 1420
反应条件
hydrogenchloride; water; acetic acid
参考文献
Journal of Organic Chemistry, , vol. 21, p. 1353,1356
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 298, p. 210,216
Journal of the Chemical Society, , p. 3315,3318
反应条件
1: diethyl ether 2: thionyl chloride 3: acetic acid; hydrochloric acid; water View Scheme
参考文献
Journal of the Chemical Society, , p. 3315,3318