N-邻苯二甲酰-L-谷氨酸合成路线 （共 20 条）
反应条件
1: diethyl ether 2: thionyl chloride 3: acetic acid; hydrochloric acid; water View Scheme
参考文献
Journal of the Chemical Society, , p. 3315,3318
反应条件
1: thionyl chloride 2: acetic acid; hydrochloric acid; water View Scheme
参考文献
Journal of the Chemical Society, , p. 3315,3318
反应条件
thiourea 0.25 h; Microwave irradiation;
参考文献
Seijas, Julio A.; Vazquez-Tato, M. Pilar; Gonzales-Bande, Cristobal; Martinez, M. Montserrat; Pacios-Lopez, Beatriz
Synthesis, 2001 , # 7 p. 999 - 1000
反应条件
in acetonitrile Decarboxylation; 30 h; Irradiation;
参考文献
Yoon, Ung Chan; Lee, Chan Woo; Oh, Sun Wha; Mariano, Patrick S.
Tetrahedron, 1999 , vol. 55, # 41 p. 11997 - 12008
反应条件
in acetonitrile Cycloaddition; 30 h; Irradiation;
参考文献
Tetrahedron, , vol. 55, # 41 p. 11997 - 12008
反应条件
1: acetic anhydride / 100 °C 2: tetrahydrofuran / 16 h / 20 °C 3: 43.8 g / hydrazine hydrate / ethanol / 4 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 36, # 2 p. 182 - 185
反应条件
1: acetic anhydride / 100 °C 2: tetrahydrofuran / 16 h / 20 °C 3: 43.8 g / hydrazine hydrate / ethanol / 4 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 36, # 2 p. 182 - 185
反应条件
acetic anhydride T=100°C;
参考文献
Craig; Bhargava; Everhart; LaBelle; Ohnsorge; Webster
Journal of Organic Chemistry, 1988 , vol. 53, # 6 p. 1167 - 1170
反应条件
1: thionyl chloride / 6 h / |Reflux; |Inert atmosphere
2: sodium amide / tetrahydrofuran / 1.5 h / -33 °C / |Inert atmosphere
View Scheme
参考文献
Varala, Ravi; Adapa, Srinivas R.
Organic Process Research and Development, 2005 , vol. 9, # 6 p. 853 - 856
反应条件
thionyl chloride in methanol
6 h; Heating / reflux;
参考文献
THE GOVERNMENT OF UNITED STATES OF AMERICA, as represented by THE SECRETARY OF THE DEPARTMENT OF HEALTH AND HUMAN SERVICES
Patent: WO2005/28436 A2, 2005 ;
Location in patent: Page/Page column 54 ;
