苯基(3-氯丙基)二氯硅烷合成路线 (共 4 条)
反应条件
dihydrogen hexachloroplatinate
参考文献
Ryan,J.W. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 3601 - 3604
参考文献
Diez-Gonzalez, Silvia; Blanco, Luis
Journal of Organometallic Chemistry, 2006 , vol. 691, # 26 p. 5531 - 5539
参考文献
Smetankina,N.P.; Miryan,N.I.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, # 6 p. 1383 - 1385,1309 - 1311
反应条件
1: 2,6-dibromohex-1-ene With magnesium; ethylene dibromide in tetrahydrofuran
T=10 - 20°C; 4 h;
2: dichloro(3-chloropropyl)phenylsilane in tetrahydrofuran
1.4 h; Heating;
参考文献
Diez-Gonzalez, Silvia; Blanco, Luis
Journal of Organometallic Chemistry, 2006 , vol. 691, # 26 p. 5531 - 5539