(Z)-11-十六碳烯-1-乙酸盐合成路线 （共 74 条）
反应条件
1: (i) Na<N(SiMe3)2>, THF, (ii) /BRN= 1746480/ 2: 9-BBN / tetrahydrofuran 3: Py / 3 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 111, # 1 p. 248 - 253
反应条件
1: pyridine / Ambient temperature 3: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4514 - 4517
反应条件
2: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4514 - 4517
反应条件
1: 93 percent / tetrahydrofuran / 48 h View Scheme
参考文献
Tetrahedron Letters, , vol. 29, # 23 p. 2777 - 2778
反应条件
1: (i) O3, (ii) NaBH4, MeOH 2: pyridine 3: (i) Mg, (ii) /BRN= 1760288/ View Scheme
参考文献
Tetrahedron Letters, , vol. No.50, p. 4851 - 4854
反应条件
1: 85 percent 2: 1) O3, 2) NaBH4 / 1) cyclohexane, MeOH 3: 92 percent / i-BuMgBr, Cp2TiCl2 4: 90 percent / pyridine View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 33, # 1 p. 25 - 30
反应条件
1: 1.) 9-borabicyclo<3.3.1>nonane, 2.) glacial acetic acid / 1.) THF, 0-5 deg C, 24 h, 2.) reflux, 9 h 2: 86 percent / pyridine / 15 h / 20 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 609 - 610
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 671 - 672
反应条件
pyridine Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Agricultural and Biological Chemistry, , vol. 44, # 2 p. 257 - 261
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) 1.) ether, 12 h, room temp., 2.) 80 deg C, 15 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1115 - 1120
参考文献
Tetrahedron Letters, , vol. 29, # 23 p. 2777 - 2778
