sodium hydride in N,N-dimethyl-formamide
T=70 - 80°C; 1 h;
参考文献
Li, Chuen; Sammes, Michael P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2193 - 2196
sodium hydride in N,N-dimethyl-formamide
T=70 - 80°C; 1 h;
参考文献
Li, Chuen; Sammes, Michael P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2193 - 2196
potassium carbonate in dimethyl sulfoxide
T=20°C; 16 h;
参考文献
Schoenebeck, Franziska; Murphy, John A.; Zhou, Sheng-Ze; Uenoyama, Yoshitaka; Miclo, Yves; Tuttle, Tell
Journal of the American Chemical Society, 2007 , vol. 129, # 44 p. 13368 - 13369
tetrabutylammomium bromide in sodium hydroxide
T=25 - 30°C; 3 h;
参考文献
Koteswar Rao, Y.; Nagarajan, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1031 - 1033
1: With lithium hexamethyldisilazane in tetrahydrofuran
T=-78°C;
2: With 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in tetrahydrofuran
T=-78 - 20°C; 3 h;
参考文献
Ni, Chuanfa; Li, Ya; Hu, Jinbo
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 6829 - 6833
Raubo, Piotr; Beer, Margaret S.; Hunt, Peter A.; Huscroft, Ian T.; London, Clare; Stanton, Josephine A.; Kulagowski, Janusz J.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 5 p. 1255 - 1258
