4,4-乙烷二氧基二苯甲醛合成路线 （共 14 条）
反应条件
potassium carbonate in acetonitrile 48 h; RefluxInert atmosphere;
参考文献
Jiang, Wei; Nowosinski, Karol; Loew, Nora L.; Dzyuba, Egor V.; Klautzsch, Fabian; Schaefer, Andreas; Huuskonen, Juhani; Rissanen, Kari; Schalley, Christoph A.
Journal of the American Chemical Society, 2012 , vol. 134, # 3 p. 1860 - 1868
反应条件
1-methyl-piperazine; sodium bis(2-methoxyethoxy)aluminium dihydride in toluene T=25°C; 3 h;
参考文献
Hagiya, Kazutake; Mitsui, Sunao; Taguchi, Hiroaki
Synthesis, 2003 , # 6 p. 823 - 828
反应条件
potassium carbonate in acetonitrile T=80°C; 16 h;
参考文献
Chan, Kin-Fai; Zhao, Yunzhe; Burkett, Brendan A.; Wong, Iris L. K.; Chow, Larry M. C.; Chan, Tak Hang
Journal of Medicinal Chemistry, 2006 , vol. 49, # 23 p. 6742 - 6759
反应条件
1: 4-(2-chloroethoxy)benzaldehyde; anabasine hydrochloride With potassium carbonate; sodium iodide in N,N-dimethyl-formamide T=60°C; 24 h; 2: oxalic acid in diethyl ether T=-20°C;
参考文献
Slyn'Ko; Tatarova; Shakirov; Shul'Ts
Chemistry of Natural Compounds, 2013 , vol. 49, # 2 p. 294 - 301
Khim. Prir. Soedin., 2013 , # 2 p. 250 - 256,7
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; Inert atmosphere;
参考文献
Ju, Chuan-Chuan; Zhang, An-Guo; Yuan, Chui-Li; Zhao, Xiao-Long; Wang, Ke-Zhi
Journal of Inorganic Biochemistry, 2011 , vol. 105, # 3 p. 435 - 443
反应条件
1: 4-hydroxy-benzaldehyde With sodium hydroxide in ethanol; water 0.5 h; Reflux; 2: ethylene dibromide in ethanol; water 4.5 h; Reflux;
参考文献
Gavrishova; Li; Sadykova; Budyka
Russian Chemical Bulletin, 2011 , vol. 60, # 7 p. 1495 - 1499
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 24 h;
参考文献
Hu, Xiao Li; Lu, Guang Nong; Chen, Lei; Yang, Ru Dong
Journal of Chemical Research - Part S, 2003 , # 6 p. 356 - 357
反应条件
1: sodium hydroxide / 0.17 h / ground in mortar 2: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere View Scheme
参考文献
Ju, Chuan-Chuan; Zhang, An-Guo; Yuan, Chui-Li; Zhao, Xiao-Long; Wang, Ke-Zhi
Journal of Inorganic Biochemistry, 2011 , vol. 105, # 3 p. 435 - 443
反应条件
1.1: N-benzyl-N,N,N-triethylammonium chloride / water / |Reflux 2.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 24 h / 60 °C 2.2: -20 °C View Scheme
参考文献
Slyn'Ko; Tatarova; Shakirov; Shul'Ts
Chemistry of Natural Compounds, 2013 , vol. 49, # 2 p. 294 - 301
Khim. Prir. Soedin., 2013 , # 2 p. 250 - 256,7
反应条件
trichlorophosphate 12 h;
参考文献
Nesunts, N. S.; Avetisyan, S. A.; Dzhagatspanyan, I. A.; Akopyan, N. E.; Mndzhoyan, O. L.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 7 p. 480 - 484
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 7 p. 801 - 806
