3-氯-4,5-二羟基苯甲醛合成路线 （共 13 条）
反应条件
boron tribromide in dichloromethane T=0 - 25°C; 4.3 h;
参考文献
Hua, Duy H.; Huang, Xiaodong; Chen, Yi; Battina, Srinivas K.; Tamura, Masafumi; Noh, Sang K.; Koo, Sung I.; Namatame, Ichiji; Tomoda, Hiroshi; Perchellet, Elisabeth M.; Perchellet, Jean-Pierre
Journal of Organic Chemistry, 2004 , vol. 69, # 18 p. 6065 - 6078
反应条件
boron tribromide in dichloromethane T=0 - 25°C; 4.3 h;
参考文献
Kansas State University Research Foundation
Patent: US6727277 B1, 2004 ;
Location in patent: Page/Page column 32 ;
反应条件
1: 88 percent / chlorine / acetic acid / 0.5 h / 25 °C 2: 94 percent / boron tribromide / CH2Cl2 / 4.3 h / 0 - 25 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 18 p. 6065 - 6078
反应条件
chlorine in water; tert-butyl alcohol
参考文献
Ohtani, Yoshito; Sumimoto, Masashi
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 9 p. 613 - 622
反应条件
chlorine in water; tert-butyl alcohol T=25°C; 0.666667 h;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 36, # 9 p. 613 - 622
反应条件
potassium carbonate; potassium iodide in acetone 25 h; Heating;
参考文献
Hua, Duy H.; Huang, Xiaodong; Chen, Yi; Battina, Srinivas K.; Tamura, Masafumi; Noh, Sang K.; Koo, Sung I.; Namatame, Ichiji; Tomoda, Hiroshi; Perchellet, Elisabeth M.; Perchellet, Jean-Pierre
Journal of Organic Chemistry, 2004 , vol. 69, # 18 p. 6065 - 6078
反应条件
1: caesium carbonate / N,N-dimethyl-formamide 2: sodium tetrahydroborate / tetrahydrofuran View Scheme
参考文献
BASF SE; BASF SCHWEIZ AG; KÖRBER, Karsten; KAISER, Florian; VEITCH, Gemma; VON DEYN, Wolfgang; BANDUR, Nina Gertrud; DICKHAUT, Joachim; NARINE, Arun; CULBERTSON, Deborah L.; NEESE, Paul; GUNJIMA, Koshi
Patent: WO2013/164295 A1, 2013 ;
反应条件
potassium carbonate in acetonitrile
T=60°C;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; ZHOU, Qun-Yong; LI, Ji-da; HUANG, Qi
Patent: WO2010/77976 A2, 2010 ;
Location in patent: Page/Page column 26 ;
WO 2010/077976 A2
反应条件
1: NaF / dimethylformamide
2: NaH / 1,2-dimethoxy-ethane
3: H2 / Pd / C
4: NaOH
View Scheme
参考文献
Jong, Ting-Ting; Williard, Paul G.; Porwoll, Joseph P.
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 735 - 736
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=60°C;
参考文献
Hadida Ruah, Sara S.; Miller, Mark T.; Bear, Brian; McCartney, Jason; Grootenhuis, Peter D. J.
Patent: US2008/9524 A1, 2008 ;
Location in patent: Page/Page column 385 ;
