7-氯-5-苯基-2-硫羰基-2,3-二氢-1,4-苯(异)二氮卓合成路线 (共 2 条)
反应条件
n-butyllithium; tetraphosphorus decasulfide in tetrahydrofuran; hexane 16 h; Heating;
参考文献
Goel, O. P.; Krolls, U.
Synthesis, 1987 , # 2 p. 162 - 164
反应条件
1: acetonitrile; H2O / 3 h / 20 °C
2: 0.33 g / sodium nitrite; AcOH / 3 h / 20 °C
View Scheme
参考文献
Del Pozo, Carlos; Macias, Alberto; Alonso, Eduardo; Gonzalez, Javier
Synthesis, 2004 , # 16 p. 2697 - 2703